首页|SPS烧结温度对ACNs/Ti复合材料组织结构与力学性能的影响

SPS烧结温度对ACNs/Ti复合材料组织结构与力学性能的影响

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通过放电等离子烧结(SPS)制备ACNs(无定形碳纳米颗粒)/Ti复合材料,并采用扫描电子显微镜、X射线衍射仪、光学显微镜以及电子万能试验机对不同烧结温度下ACNs/Ti复合材料的显微组织、相组成及力学性能进行表征.结果表明,较低烧结温度(800℃)下,未反应的ACNs虽然会对复合材料的强度有所贡献,但其与基体的界面结合较弱,会导致复合材料塑性严重下降.较高烧结温度(1000℃)下,与基体充分反应的TiC颗粒过度生长后尺寸较大,这一现象会造成材料强度下降.当烧结温度为 900℃时,ACNs与Ti基体完全反应生成TiC颗粒,这种细小弥散的TiC沿着基体颗粒周围分布形成了准连续网状结构,此时ACNs/Ti复合材料具有最佳的强塑性匹配,其抗拉强度、屈服强度、延伸率分别为 648.19 MPa、551.02 MPa、36.19%.
Effect of SPS Sintering Temperature on Organization and Mechanical Properties of ACNs/Ti Composite
ACNs(amorphous carbon nanoparticles)/Ti composites were prepared by spark plasma sintering(SPS),and the microstructures,phase compositions and mechanical properties of ACNs/Ti composites at different sintering temperatures were characterised using scanning electron microscope,X-ray diffractometer,optical microscope and electronic universal testing machine.The results show that at lower sintering temperature(800℃),although the unreacted ACNs will contribute to the strength of the composites,the weak interfacial bonding with the matrix will lead to serious decrease in the plasticity of the composites.At higher sintering temperature(1000℃),the TiC particles that are fully reacted with the matrix are larger in size after overgrowth,and this phenomenon causes a decrease in the strength of the material.When the sintering temperature is 900℃,the ACNs fully react with the Ti matrix to produce TiC particles.The TiC particles are distributed along the perimeter of the matrix particles,forming a quasi-continuous mesh structure,and the ACNs/Ti composite has the best strong-plasticity match,the tensile strength,yield strength and elongation are 648.19 MPa,551.02 MPa and 36.19%,respectively.

ACNs/Ti compositespark plasma sinteringmicrostructuremechanical properties

赵宁、王海丽、张媚、孙国栋

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西安石油大学 材料科学与工程学院,陕西 西安 710065

西安稀有金属材料研究院有限公司,陕西 西安 710016

ACNs/Ti复合材料 放电等离子烧结 显微组织 力学性能

陕西省创新能力支撑计划陕西省重点研发计划

2023KJXX-0962024GX-YBXM-355

2024

钛工业进展
中国有色金属工业协会钛锆铪分会 西北有色金属研究院

钛工业进展

CSTPCD
影响因子:0.2
ISSN:1009-9964
年,卷(期):2024.41(2)
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