钛工业进展2024,Vol.41Issue(5) :38-41.

ICP-AES法测定钛合金用AlVSnCuFe中间合金中常量元素含量

ICP-AES Method for Constant Elements in AlVSnCuFe Intermediate Alloy for Titanium Alloys

徐兴 杨平平 刘雷雷 周恺
钛工业进展2024,Vol.41Issue(5) :38-41.

ICP-AES法测定钛合金用AlVSnCuFe中间合金中常量元素含量

ICP-AES Method for Constant Elements in AlVSnCuFe Intermediate Alloy for Titanium Alloys

徐兴 1杨平平 2刘雷雷 2周恺2
扫码查看

作者信息

  • 1. 中国商飞上海飞机设计研究院,上海 200126;大型客机集成技术与模拟飞行全国重点实验室,上海 200126
  • 2. 西安汉唐分析检测有限公司,陕西 西安 710201
  • 折叠

摘要

采用电感耦合等离子体原子发射光谱仪(ICP-AES),在最佳仪器参数情况下,通过对溶解酸种类、称样量与定容体积、分析谱线、短时稳定性、共存元素干扰、工作曲线等进行研究,优化了试验条件,建立了钛合金用AlVSnCuFe中间合金中常量元素含量的ICP-AES测定方法.该方法中Al和V元素测定范围为 10.00%~50.00%,Fe和Cu元素测定范围为 2.00%~10.00%,Sn元素测定范围为 4.00%~20.00%;加标回收率为 97.5%~103.2%,精密度(RSD)不大于 2.5%.该方法具有检测准确度和稳定性好、效率高等特点,有效解决了 AlVSnCuFe中间合金中常量元素的检测问题.

Abstract

Under the optimal instrument parameters,the inductively coupled plasma atomic emission spectrometry(ICP-AES)was used to optimize the experimental conditions by studying the types of dissolved acids,sample size and constant volume,analytical spectral lines,short-term stability,coexisting element interference,standard solutions for working curves,etc.,and an ICP-AES method for constant elements in AlVSnCuFe intermediate alloy for titanium alloys was established.This method is suitable for the determination of constant elements in intermediate alloy,and has the characteristics of good test accuracy,high efficiency,and good stability.The testing range for Al and V elements is 10.00%to 50.00%,the testing range for Fe and Cu elements is 2.00%to 10.00%,and the testing range for Sn element is 4.00%to 20.00%.The spiked recovery rate is 97.5%to 103.2%,and the precision RSD is not more than 2.5%.This method effectively solves the problem of detecting constant elements in AlVSnCuFe intermediate alloy.

关键词

钛合金/中间合金/AlVSnCuFe/电感耦合等离子体原子发射光谱法

Key words

titanium alloy/intermediate alloy/AlVSnCuFe/inductively coupled plasma atomic emission spectroscopy

引用本文复制引用

基金项目

陕西省科技资源开放平台项目(2024CX-GXPT-28)

出版年

2024
钛工业进展
中国有色金属工业协会钛锆铪分会 西北有色金属研究院

钛工业进展

CSTPCD
影响因子:0.2
ISSN:1009-9964
段落导航相关论文