首页|超声波辅助制备河蟹酶解液微胶囊乳液的工艺优化

超声波辅助制备河蟹酶解液微胶囊乳液的工艺优化

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为进一步提高河蟹酶解液(River crab enzymolysis liquid,RCEL)微胶囊乳液的成囊效果,本试验在前期复凝聚法研究结果的基础上采用超声波辅助工艺制备RCEL微胶囊乳液,复凝聚法的壁材分别为明胶-海藻酸钠和明胶-CMC-Na,选择超声功率、超声时间和超声温度为考察因素,以香气感官评分为评价指标,采用L9(34)正交试验优选超声波辅助工艺参数.试验结果表明:壁材为明胶-海藻酸钠时的超声波最佳条件为:超声功率 50%(×700W)、超声时间 20 min、超声温度30℃;壁材为明胶-CMC-Na时微胶囊最佳试验条件为:功率 40%(×700W)、时间 30 min、温度30℃.在这两个条件下得到 RCEL 微胶囊形状规则呈圆球形,且微胶囊数量多,但在香气感官评分上,壁材为明胶-海藻酸钠时复热后蟹味浓郁,而壁材为明胶-CMC-Na复热后的蟹味较弱.综上,采用复凝聚法,以明胶-海藻酸钠为璧材,进行先乳化后超声处理制备RCEL微胶囊乳液,此时的成囊效果最佳,且复热后蟹味最浓.
Optimization of ultrasonic-assisted preparation technology of microcapsule emulsion from hydrolysate of crab
In order to further improve the microencapsulation effect of river crab enzymolysis liquid(RCEL)microcapsule emulsion,based on the previous research results of complex coacervation method,ultrasonic-assisted technology was used to prepare RCEL microcapsule emulsion.The wall materials of complex coacervation method were gelatin-sodium alginate and gelatin-CMC-Na,respectively.Ultrasonic power,ultrasonic time and ultrasonic temperature were selected as the investigation factors,aroma sensory score was used as the evaluation index,and L9(34)was adopted.The results showed that the optimum ultrasonic conditions when the wall material was gelatin-sodium alginate were as follows:ultrasonic power 50%(×700W),ultrasonic time 20 min and ultrasonic temperature 30℃;when the wall was gelatin-CMC-Na,the best experimental conditions of microcapsules were:power 40%(×700W),time 30min,temperature 30℃.Under those two conditions,RCEL microcapsules were round and regular in shape,and the number of microcapsules was large.However,on the sensory evaluation of aroma,the crab flavor after reheating with gelatin-sodium alginate as the wall material was strong,while the crab flavor after reheating with gelatin-CMC-Na as the wall material was weak.To sum up,when RCEL microcapsule emulsion was prepared by complex coacervation method,with gelatin-sodium alginate as the wall material,emulsification followed by ultrasonic treatment,the encapsulation effect was the best,and the crab flavor was the strongest after reheating.

ultrasoundcomplex coacervation methodmicrocapsulationcrab flavor

符慧靖、李彦、沈德熊、马俪珍

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天津农学院 食品科学与生物工程学院 天津 300392

可可溢香(江苏)味业有限公司 江苏 兴化 225700

超声波 复凝聚法 微胶囊 蟹味

天津市淡水养殖产业技术体系建设项目创新团队水产品加工岗位项目

ITTFRS2021000-012

2024

天津农学院学报
天津农学院

天津农学院学报

影响因子:0.612
ISSN:1008-5394
年,卷(期):2024.31(2)
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