特种铸造及有色合金2024,Vol.44Issue(9) :1232-1236.DOI:10.15980/j.tzzz.2024.09.014

热处理过程中压力对Mg-14Gd-1Zn-0.4Zr合金组织与力学性能的影响

Effects of Pressure on Microstructure and Mechanical Properties of Mg-14Gd-1Zn-0.4Zr Alloy during Heat Treatment

吴海 王阳阳 张旻 杨力祥 董喜旺 华溪如 肖旅
特种铸造及有色合金2024,Vol.44Issue(9) :1232-1236.DOI:10.15980/j.tzzz.2024.09.014

热处理过程中压力对Mg-14Gd-1Zn-0.4Zr合金组织与力学性能的影响

Effects of Pressure on Microstructure and Mechanical Properties of Mg-14Gd-1Zn-0.4Zr Alloy during Heat Treatment

吴海 1王阳阳 2张旻 2杨力祥 1董喜旺 1华溪如 1肖旅1
扫码查看

作者信息

  • 1. 上海航天精密机械研究所,上海 201600
  • 2. 上海航天技术研究院,上海 201600
  • 折叠

摘要

针对铸造稀土镁合金固溶处理过程中普遍存在的合金元素充分固溶与晶粒长大间的矛盾,从压力角度探索其对合金元素固溶过程的影响.对比研究了真空与常压固溶处理后Mg-14Gd-1Zn-0.4Zr合金的组织与力学性能,以及峰时效态的力学性能,并讨论了压力对原子固溶过程的影响机制.结果表明,Mg-14Gd-1Zn-0.4Zr合金铸态组织主要由α-Mg、(Mg,Zn)3Gd、14H型LPSO相组成.常压480℃×20 h固溶处理后LPSO相消失,有少量(Mg,Zn)3Gd残留.常压500℃×20 h与真空480℃×20 h固溶处理后,LPSO相均消失且基本无(Mg,Zn)3Gd相残留,但真空条件下晶粒未显著长大,强塑性均有所提升;二者在 225℃时效处理的峰时效时间均为 24 h,后者的抗拉强度与伸长率提升明显,抗拉强度为(360.5±1.2)MPa,屈服强度为(234.6±0.8)MPa,伸长率为(5.2±0.3)%.当压力降低至真空时,合金原子的扩散系数增加,提高了固溶效率;在较低固溶温度下也可实现Gd、Zn原子固溶,同时减缓了晶粒长大,因此促进了合金综合强塑性提升.

Abstract

In view of the contradiction between sufficient solid solution of alloying elements and grain growth,the effects of pressure on solid solution process of alloying elements were investigated.The microstructure and mechanical properties of Mg-14Gd-1Zn-0.4Zr alloy after vacuum and atmospheric solution treatment as well as the mechanical properties of alloys in peak-aging state were analyzed.The influence mechanism of pressure on atomic solution process was described.The results indicate that the microstructure of as-cast Mg-14Gd-1Zn-0.4Zr alloy is mainly composed of α-Mg,(Mg,Zn)3Gd,14H LPSO phases.After solution treatment at 480℃×20 h at normal pressure,LPSO phase disappears and a small amount of(Mg,Zn)3Gd remains.After solution treatment at 500℃×20 h at normal pressure and 480℃×20 h at vacuum conditions,LPSO phase disappears and absence of residual(Mg,Zn)3Gd phase can be observed,however the grain size is coarsened slightly under vacuum condition,and the strength and plasticity are increased.The peak aging time of both alloys at 225℃is 24 h,and the tensile strength and elongation of the latter are significantly improved,with the tensile strength of(360.5±1.2)MPa,yield strength of(234.6±0.8)MPa,and elon-gation of(5.2±0.3)%.When the pressure is reduced to vacuum,the diffusion coefficient of atoms is increased and the solution efficiency is improved.Solid solution of Gd and Zn atoms can be achieved at a lower solution temperature,and the grain growth is retarded,thus improving overall strength and toughness.

关键词

压力/热处理/Mg-14Gd-1Zn-0.4Zr合金/力学性能

Key words

Pressure/Solution Treatment/Mg-14Gd-1Zn-0.4 Zr Alloy/Mechanical Properties

引用本文复制引用

基金项目

国家自然科学基金资助项目(U2037601)

出版年

2024
特种铸造及有色合金
中国机械工程学会铸造分会

特种铸造及有色合金

CSTPCD北大核心
影响因子:0.481
ISSN:1001-2249
段落导航相关论文