首页|EDS和EBSD联用法分析高温合金和高强度钢的物相

EDS和EBSD联用法分析高温合金和高强度钢的物相

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为了分析高温合金和高强度钢的物相,采用能谱仪(EDS)和电子背散射衍射仪(EBSD)联用法,鉴定镍基母合金的非金属夹杂物以及区分300M低合金高强度钢的氧化层物相.结果表明,镍基母合金菊池带中心线倾角的平均角度偏差(MAD)为0.79°,经过与数据库中各选定物相的模拟花样进行比对,非金属夹杂物鉴定为Al2O3.300M钢通过离子抛光后,利用EBSD技术能够区分氧化层中的物相并确定其分布情况,大部分是Fe3O4,其次是Fe2O3,FeO含量极少.
Analysis of phases in superalloy and high-strength steel by combination of EDS and EBSD
In order to analyze the phases of superalloy and high-strength steel,the combination method of EDS and EBSD was adopted.The non-metallic inclusions in nickel-based master alloy were identified,and the oxide layer phases of 300M low-alloy high-strength steel were distinguished.The result showed that the mean angular deviation(MAD)of the center line inclination of the nickel-based master alloy Kikuchi band was 0.79°.The non-metallic inclusion was identified as Al2O3 by comparison with the simulation bands of selected phases in the database.After ion polishing,the phases in the 300 M steel oxide layer and their distribution could be distinguished and determined by the EBSD technology.Most phases were Fe3O4 followed by Fe2O3,and the content of FeO was extremely low.

nickel-based master alloy300M steelelectron backscatter diffraction(EBSD)phase analysis

唐凯明、王博、宁新伟、王维、朱杰、徐中华

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江苏隆达超合金航材有限公司,江苏无锡 214105

日立科学仪器(北京)有限公司上海分公司,上海 200235

镍基母合金 300M钢 电子背散射衍射技术 物相分析

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2022YFB3705002G20221001

2024

物理测试
中国钢研科技集团有限公司

物理测试

影响因子:0.363
ISSN:1001-0777
年,卷(期):2024.42(5)