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重铬酸盐法测定水中化学需氧量新标准不确定度评定

Uncertainty evaluation of new standard for determination of chemical oxygen demand in water by using bichromate method

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新标准《水质化学需氧量的测定重铬酸盐法》 (HJ 828—2017) 代替旧标准GB 11914-89), 文中以新标准方法进行检测.分析该方法不确定度来源, 考虑到测量器具、标准溶液、环境条件和测量重复性等因素对化学需氧量测量不确定度有影响, 通过具体实验得出了此次化学需氧量测定结果为:212 mg/L, 其合成不确定度为:2.25 mg/L, 扩展不确定度为:4.50 mg/L.
Water quality-Determination of the chemical oxygen demand-Dichromate method (HJ 828-2017 instead of GB11914-89) was tested by a new standard method. The analysis method of uncertainty sources, taking into account the measuring instrument, standard solution, environmental conditions and measurement repeatability of COD measurement uncertainty influence, through specific experimental results of the determination of some chemical oxygen demand: were 212 mg/L, the synthesis uncertainty was 2. 25 mg/L and extension uncertainty was 4. 50 mg/L.

potassium bichromate methodCODuncertaintyevaluation

孙佳、仇欣

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镇江市环境监测中心站,江苏镇江 212009

江苏环球嘉惠环境科学研究有限公司,江苏镇江 212004

重铬酸钾法 化学需氧量 不确定度 评定

2018

污染防治技术
中国环境科学学会 江苏省环境科学学会

污染防治技术

ISSN:
年,卷(期):2018.31(4)
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