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玉米秸秆微晶纤维素的制备及其性质

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以玉米秸秆为原料,研究其提取制备微晶纤维素的工艺及产品性能.探讨酸解温度、硫酸体积分数、酸解时间对微晶纤维素聚合度及得率的影响,并对微晶纤维素的理化性质进行了分析.结果表明:玉米秸秆微晶纤维素最佳制备工艺条件为:反应温度85 ℃,硫酸体积分数8%,水解时间90 min,此时制得微晶纤维素聚合度为292,纯度92.6%,得率76.48%,结晶度为74.5%.在此条件下,玉米秸秆微晶纤维素在保留形态结构的同时具有较高的结晶度和热稳定性,具备较好的应用性能和价值.
Preparation and Properities of Microcrystalline Cellulose from Corn Stalk
Corn stalk was used to prepare microcrystalline cellulose (MCC) and product properties were studied.The optimal parameters for MCC preparation were founded to be 8% (w/w) of H2SO4,hydrolyzing time 90 min and temperature 85 ℃,which resulted in a polymerization degree of 292,a content of 92.6%,a yield of 76.48% and a crystallinity of 74.5% for cellulose.Under these conditions,MCC retained the original morphological structure with high crystallinity and thermal stability,thus possessing favorable properties for future use.

corn stalkmicrocrystalline cellulosedegree of polymerization

张冬丽、程力、顾正彪、洪雁、李兆丰

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江南大学食品学院,江苏无锡214122

食品科学与技术国家重点实验室,江苏无锡214122

江南大学食品安全与营养协同创新中心,江苏无锡214122

玉米秸秆 微晶纤维素 聚合度

2016

食品与生物技术学报
江南大学

食品与生物技术学报

CSTPCDCSCD北大核心
影响因子:0.674
ISSN:1673-1689
年,卷(期):2016.35(10)
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