食品与生物技术学报2024,Vol.43Issue(6) :119-127.DOI:10.12441/spyswjs.20230422001

GC-IMS、GC-MS技术分析龙蒿挥发性成分

Analysis of Volatile Components of Tarragon Based on GC-IMS and GC-MS

后春静 贾爽 柒梦阳 蔡文凯 户新宇 郭勤
食品与生物技术学报2024,Vol.43Issue(6) :119-127.DOI:10.12441/spyswjs.20230422001

GC-IMS、GC-MS技术分析龙蒿挥发性成分

Analysis of Volatile Components of Tarragon Based on GC-IMS and GC-MS

后春静 1贾爽 1柒梦阳 1蔡文凯 2户新宇 3郭勤1
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作者信息

  • 1. 新疆理工学院能源化工工程学院,新疆阿克苏 843100
  • 2. 温州大学温州市微纳米电器件重点实验室,浙江温州 325035
  • 3. 新疆理工学院能源化工工程学院,新疆阿克苏 843100;温州大学温州市微纳米电器件重点实验室,浙江温州 325035
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摘要

采用气相色谱-离子迁移谱联用(gas chromatography-ion mobility spectrometry,GC-IMS)和气相色谱-质谱联用(gas chromatography-mass spectrometry,GC-MS)技术探究了龙蒿挥发性成分.结果表明,在天山南坡龙蒿生长发育过程中,精油逐渐积累.GC-IMS检测结果表明,龙蒿叶中含有35种挥发性有机化合物(volatile organic compounds,VOCs),其碳链在C2~C10,主要包括萜烯类6种、醛类12种、醇类4种、呋喃类1种、酯类3种、酮类5种、其他物质4种,且各挥发性成分存在差异.GC-MS检测结果表明,龙蒿精油中含有挥发性有机化合物54种,其碳链在C7~C32,其中含有萜烯类16种、醇类12种、酯类9种、酚类4种、醛类2种等,GC-MS检测出的有机化合物种类相对较多,相对分子质量较大.GC-MS和GC-IMS技术互为补充,可以更加全面获得龙蒿挥发性成分的综合信息,为龙蒿及其精油的开发利用和分析检测提供新思路.

Abstract

This study utilized gas chromatography-ion mobility spectrometry(GC-IMS)and gas chromatography-mass spectrometry(GC-MS)to investigate the volatile components of tarragon.The results indicated that essential oil accumulation was a gradual process during the growth and development of tarragon on the southern slope of the Tianshan mountains.The detection results of GC-IMS showed that tarragon leaves contained 35 volatile organic compounds(VOCs)with carbon chains ranging from C2 to C10,mainly including 6 terpenes,12 aldehydes,4 alcohols,1 furan,3 esters,5 ketones,and 4 other substances,with significant differences among them.The detection of GC-MS identified 54 volatile organic compounds in tarragon essential oil,with carbon chains ranging from C7 to C32,including 16 terpenes,12 alcohols,9 esters,4 phenols,and 2 aldehydes etc.GC-MS detected a relatively large number of species with higher relative molecular weight.The complementary use of GC-MS and GC-IMS technologies can provide comprehensive information on the volatile components of tarragon,offering new research perspectives for the development,utilization,analysis and detection of tarragon and its essential oils.

关键词

龙蒿/挥发性成分/气相色谱-离子迁移谱/气相色谱-质谱

Key words

tarragon/volatile components/gas chromatography-ion mobility spectrometry/gas chromatography-mass spectrometry

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基金项目

新疆维吾尔自治区自然科学基金青年科学基金项目(2023D01C221)

新疆维吾尔自治区自然科学基金青年科学基金项目(2021D01B42)

科技兴阿项目(2021-23)

新疆维吾尔自治区天山创新团队计划项目(2021D14013)

大学生创新创业训练计划项目(S202313558008)

大学生创新创业训练计划项目(S202313558013)

大学生创新创业训练计划项目(JWSC2022156)

温州市科协项目(kjfw04)

温州市科协项目(kjfw37)

出版年

2024
食品与生物技术学报
江南大学

食品与生物技术学报

CSTPCD北大核心
影响因子:0.674
ISSN:1673-1689
参考文献量7
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