现代化工2024,Vol.44Issue(4) :228-232.DOI:10.16606/j.cnki.issn0253-4320.2024.04.043

污水中十二烷基磺酸钠快速检测试纸的研制

Establishment of rapid test paper for detection of sodium dodecyl sulfonate in sewage

赵文青 解清杰 董进波 王超 林华星
现代化工2024,Vol.44Issue(4) :228-232.DOI:10.16606/j.cnki.issn0253-4320.2024.04.043

污水中十二烷基磺酸钠快速检测试纸的研制

Establishment of rapid test paper for detection of sodium dodecyl sulfonate in sewage

赵文青 1解清杰 1董进波 2王超 1林华星1
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作者信息

  • 1. 江苏大学环境与安全工程学院,江苏 镇江 212013
  • 2. 江苏满江春城市规划设计研究有限责任公司,江苏 镇江 212008
  • 折叠

摘要

基于结晶紫与十二烷基磺酸钠在pH为7.00的缓冲溶液下发生反应,建立了一种十二烷基磺酸钠的快速检测试纸来判断污水中是否含有阴离子表面活性剂.结果发现,当浸渍1 mg/L结晶紫溶液的试纸和pH为7.00的缓冲溶液混合时(结晶紫溶液与缓冲溶体积比是3∶1)显色更明显;十二烷基磺酸钠浓度与显色深浅呈正比.该十二烷基磺酸钠检测试纸的检测最低值为0.05 mg/L,最高值为2 mg/L.配制样品测定结果的相对误差范围为1.167%~4.233%,表明该方法具有良好的准确性.

Abstract

Based on the reaction between crystal violet and sodium dodecyl sulfonate in a buffer solution with a pH of 7.00,a rapid test paper for sodium dodecyl sulfonate is developed to determine whether wastewater contains anionic surfactants or not.The results show that the color will be more pronounced when the test paper dipped with 1 mg·L-1 crystal violet solution is mixed with the buffer solution with a pH of 7.00,under a volume ratio of 3∶1.The concentration of sodium dodecyl sulfonate is proportional to the color rendering depth,and the color of the solution changes from colorless to light rose red to rose red to purple red.The lowest and highest detection values of the sodium dodecyl sulfonate test paper are 0.05 mg·L-1 and 2 mg·L-1,respectively.The relative error ranges from 1.167%to 4.233%for detection results of prepared samples,showing a good accuracy.

关键词

十二烷基磺酸钠/结晶紫/标准比色卡/试纸检测/试纸浸渍液

Key words

sodium dodecyl sulfonate/crystal violet/standard colorimetric card/detection by test paper/dipping solution for test paper

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基金项目

镇江市科技计划(社会发展)(SH2021012)

出版年

2024
现代化工
中国化工信息中心

现代化工

CSTPCDCSCD北大核心
影响因子:0.553
ISSN:0253-4320
参考文献量20
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