首页|25%唑·氰氟乳油高效液相色谱分析

25%唑·氰氟乳油高效液相色谱分析

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建立高效液相色谱法,采用紫外检测器和CHIRALCE OD-H柱,以正己烷、乙醇(95∶5,V/V)为流动相,在238 nm波长下进行25%唑·氰氟乳油中有效成分的含量测定.结果表明,唑酰草胺和氰氟草酯的线性相关系数分别为0.999 1和0.999 3,变异系数分别为1.03%和0.58%,平均回收率分别为99.82%、99.54%.此方法的精密度及准确度良好,均符合分析标准,可用于复配产品中的唑酰草胺和氰氟草酯的检测分析.
Analysis of metamifop·cyhalofop-butyl 25%EC by HPLC
A quantitative analysis method was introduced for the determination of metamifop·cyhalofop-butyl 25%EC by HPLC on CH1RALCE OD-H column with ultraviolet detector at 238 nm.The mobile phase was made up of n-hexane and ethanol(95∶5,V/V).The results showed that the linear correlation coefficients of metamifop and cyhalofop-butyl were 0.9991 and 0.999 3,the coefficients of variation were 1.03%and 0.58%,and the average recoveries were 99.82%and 99.54%,respectively.The precision and accuracy of the method were good.It could be used for the determination of metamifop and cyhalofop-butyl in compound products effectively.

metamifopcyhalofop-butylHPLCanalysis

王娟、马超、张喆、赵宜君、徐军、陈昶

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河北中保绿农作物科技有限公司,河北廊坊 065000

中国农业科学院植物保护研究所,北京 100193

唑酰草胺 氰氟草酯 高效液相色谱 分析

2024

现代农药
江苏省农药协会 江苏省农药研究所股份有限公司 江苏省农药科技信息站

现代农药

CSTPCD
影响因子:0.471
ISSN:1671-5284
年,卷(期):2024.23(1)
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