现代农药2024,Vol.23Issue(4) :44-46.DOI:10.3969/j.issn.1671-5284.2024.04.008

30%虫螨腈·氯虫苯甲酰胺悬浮剂高效液相色谱分析

Analysis of chlorfenapyr·chlorantraniliprole 30%SC by HPLC

白亮 马超 赵宜君 张喆 张立群 赵淑元 徐军 陈昶
现代农药2024,Vol.23Issue(4) :44-46.DOI:10.3969/j.issn.1671-5284.2024.04.008

30%虫螨腈·氯虫苯甲酰胺悬浮剂高效液相色谱分析

Analysis of chlorfenapyr·chlorantraniliprole 30%SC by HPLC

白亮 1马超 1赵宜君 2张喆 1张立群 1赵淑元 1徐军 2陈昶2
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作者信息

  • 1. 河北中保绿农作物科技有限公司,北京 100193
  • 2. 河北中保绿农作物科技有限公司,北京 100193;中国农业科学院植物保护研究所,北京 100193
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摘要

建立液相色谱测定30%虫螨腈·氯虫苯甲酰胺悬浮剂的分析方法.以甲醇+水(体积比80∶20)为流动相,使用C18色谱柱,在254 nm波长下检测.试验结果表明:虫螨腈和氯虫苯甲酰胺的相关系数分别为0.999 5和0.999 2,标准偏差分别为0.02和0.02,相对标准偏差分别为0.1%和0.2%,平均回收率分别为99.64%和99.31%.方法简便快捷,精密度和准确度高,可有效用于复配产品中虫螨腈和氯虫苯甲酰胺的定量分析检测.

Abstract

An analytical method of chlorfenapyr·chlorantraniliprole 30%SC was established by HPLC.Chlorfenapyr and chlorantraniliprole were determined on stainless steel column C i8,using methanol+water(volume ratio of 80∶20)as the mobile phase,at the wavelength of 254 nm.The results showed that the linear correlation coefficients of chlorfenapyr and chlorantraniliprole were 0.999 5 and 0.999 2,the standard deviations were 0.02 and 0.02,the relative standard deviations were 0.1%and 0.2%,and the average recoveries were 99.64%and 99.31%,respectively.The method was simple and rapid,with high accuracy and precision,good linear correlation.It could be used for the quantitative analysis of chlorfenapyr and chlorantraniliprole in compound products.

关键词

虫螨腈/氯虫苯甲酰胺/高效液相色谱/分析

Key words

chlorfenapyr/chlorantraniliprole/HPLC/analysis

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基金项目

国家重点研发计划项目(2022YFD1400303)

出版年

2024
现代农药
江苏省农药协会 江苏省农药研究所股份有限公司 江苏省农药科技信息站

现代农药

CSTPCD
影响因子:0.471
ISSN:1671-5284
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