首页|采用扫描电子显微镜研究防护蜡在橡胶中析出形貌的影响因素

采用扫描电子显微镜研究防护蜡在橡胶中析出形貌的影响因素

Study on Influence Factors of Protective Wax Precipitation Morphology in Compounds by Scanning Electron Microscopy

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利用扫描电子显微镜表征天然橡胶/顺丁橡胶胎侧胶中不同种类防护蜡在不同停放条件下析出的蜡膜形貌,研究蜡膜形貌受环境温湿度的影响规律.结果表明:防护蜡组成中低碳数正构烷烃在4℃低温和室温下易析出片状形貌蜡膜,高碳数正构和异构烷烃在40℃高温下易析出聚集球状形貌蜡膜,40与20℃交替变温对高碳数烷烃析出有促进作用,易形成整片连续的聚集球状蜡膜;高温下湿度变化对蜡膜形貌的影响不大.
The morphology of wax films precipitated from different kinds of protective waxes in natural rubber/butadiene rubber sidewall compounds under different storage conditions was characterized by scanning electron microscopy,and the influences of environmental temperature and humidity on the morphology of wax films were studied.The results showed that the low-carbon number normal paraffins in the protective wax composition were easy to precipitate flake-shaped wax film at low temperature(4℃)and room temperature,and the high-carbon number normal paraffins and isoparaffins were easy to precipitate aggregated spherical wax film at 40℃.The alternation of temperatures from 40 to 20℃promoted the precipitation of high-carbon number paraffins,facilitating the formation of a continuous aggregated spherical wax film.Humidity variation at high temperature had little effect on the morphology of wax film.

scanning electron microscopyprotective waxsidewall compoundcarbon number distributionwax film morphologystorage conditiontemperature

郑丽娜、齐生凯、雷蕾、吴爱芹、刘爱芹

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思通检测技术有限公司,山东 青岛 266045

怡维怡橡胶研究院,山东 青岛 266045

青岛科技大学 高分子科学与工程学院,山东 青岛 266042

扫描电子显微镜 防护蜡 胎侧胶 碳数分布 蜡膜形貌 停放条件 温度

2025

橡胶科技
北京橡胶工业研究设计院 全国橡胶工业信息总站

橡胶科技

影响因子:0.104
ISSN:1672-125X
年,卷(期):2025.23(1)