香料香精化妆品2024,Issue(1) :132-137.DOI:10.20099/j.issn.1000-4475.2023.0006

烈香杜鹃精油特征香气成分的GC-O-MS分析及其在卷烟中的应用

GC-O-MS Analysis of Characteristic Aroma Components of Rhododendron Anthopogonoides Oil and Its Application to Cigarette

张学建 吴雷 常丹丹 丁为 崔韬 申屠洪钎 朱笛恺 王益明 杨涓 杨庆国 朱宇 陶飞燕
香料香精化妆品2024,Issue(1) :132-137.DOI:10.20099/j.issn.1000-4475.2023.0006

烈香杜鹃精油特征香气成分的GC-O-MS分析及其在卷烟中的应用

GC-O-MS Analysis of Characteristic Aroma Components of Rhododendron Anthopogonoides Oil and Its Application to Cigarette

张学建 1吴雷 2常丹丹 2丁为 3崔韬 3申屠洪钎 3朱笛恺 2王益明 2杨涓 3杨庆国 3朱宇 3陶飞燕1
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作者信息

  • 1. 四川中烟工业有限责任公司,四川成都 610066;四川三联新材料有限公司,四川成都 610041
  • 2. 四川三联新材料有限公司,四川成都 610041
  • 3. 四川中烟工业有限责任公司,四川成都 610066
  • 折叠

摘要

采用水蒸气蒸馏法制备烈香杜鹃精油,并运用气相色谱-质谱联用技术(GC-MS)分析烈香杜鹃精油的挥发性成分,共鉴定出 69 种化合物.同时,通过香气强度法结合气相色谱-嗅闻技术(GC-O)分析,发现 9 种香气强度大于 3 的特征香气成分:叶醇、白菖烯、α-瑟林烯、乙酸苯乙酯、大根香叶烯B、苄基丙酮、2-丁烯基苯、苍术酮和吉马酮;其中 3 种香气强度大于5 的苄基丙酮、叶醇和α-瑟林烯为关键香气成分.将烈香杜鹃精油进行卷烟滤棒添加试验,发现其能赋予卷烟清香、甜香和花香,与烟气协调,细腻柔和烟气,并且增加甜感.

Abstract

The essential oil of Rhododendron anthopogonoides was prepared by steam distillation,and the volatile components of Rhododendron anthopogonoides oil were analyzed by gas chromatography-mass spectrometry(GC-MS),and a total of sixty-nine compounds were identified.Meanwhile,nine characteristic aroma components with aroma intensity(AI)values greater than 3 were characterized by AI method and gas chromatograph-olfactometry(GC-O)analysis:leaf alcohol,(+)-calarene,α-selinene,phenethyl acetate,germacrene B,benzyl acetone,2-butenyl-benzene,atractyline and germacrone.Three of them,benzyl acetone,leaf alcohol and α-selinene were key aroma components with AI value>5.Then,the cigarette flavoring experiment was carried out with Rhododendron anthopogonoides oil injected into cigarette filter.The results showed that Rhododendron anthopogonoides oil could enhance the refreshing,sweet and flower aroma characteristics,harmonize with the smoke,delicate and soften the smoke,and increase the sweetness.

关键词

烈香杜鹃/气相色谱-嗅闻-质谱联用技术/特征香气成分/卷烟加香

Key words

Rhododendron anthopogonoides/gas chromatography-olfactometry-mass spectrometry(GC-O-MS)/characteristic aroma component/cigarette flavoring

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出版年

2024
香料香精化妆品
上海香料研究所

香料香精化妆品

CSTPCD
影响因子:0.341
ISSN:1000-4475
参考文献量6
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