稀有金属材料与工程2024,Vol.53Issue(2) :424-434.DOI:10.12442/j.issn.1002-185X.20230020

变形量对半固态CuSn10合金组织和性能的影响

Effects of Deformation on the Microstructure and Properties of Semi-solid CuSn10 Alloys

文科 李永坤 周荣锋 殷新华 熊文韬 刘程祥 张亚真
稀有金属材料与工程2024,Vol.53Issue(2) :424-434.DOI:10.12442/j.issn.1002-185X.20230020

变形量对半固态CuSn10合金组织和性能的影响

Effects of Deformation on the Microstructure and Properties of Semi-solid CuSn10 Alloys

文科 1李永坤 2周荣锋 2殷新华 1熊文韬 1刘程祥 1张亚真1
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作者信息

  • 1. 昆明理工大学材料科学与工程学院,云南 昆明 650093
  • 2. 昆明理工大学材料科学与工程学院,云南 昆明 650093;昆明理工大学城市学院,云南 昆明 650051
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摘要

材料的组织形态直接影响零件的性能,采用自主研发的熔体约束诱导形核半固态制浆装置制备CuSn10半固态浆料并流变挤压成薄板,然后在350 ℃下轧制变形,研究变形量对微观组织和性能的影响.结果表明,随着变形量增加,变形板件内部缩松缩孔等铸造缺陷逐渐减少减小、晶粒呈现压缩拉长趋势、平均晶粒厚度从初始未变形时30.58 μm到变形量ε=0.4时的22.12 μm.随变形量的加大在初生相内部产生的形变孪晶数量逐渐增加.在变形量从ε=0增加到ε=0.4的过程中,CuSn10合金组织内小角度晶界占比逐渐占优,引入了大量的亚结构和位错密度.在变形量ε=0.4时,可以发现极图{110}和{111}存在[101]、[111]和[001]织构.在板材力学性能方面,板材的屈服强度、抗拉强度和硬度不断增加;但塑性呈现下降的趋势.变形量ε=0.4时,其屈服强度、抗拉强度和布氏硬度(HBW)分别达到了 443 MPa、554 MPa、1901.2 MPa,相较于初始未变形薄板其屈服强度、抗拉强度和硬度分别提高了 106.1%、66.4%、41.6%,延伸率降低至0.82%.半固态CuSn10合金在变形过程中随变形量的增加强度、硬度不断提高、塑性持续降低,这主要是归功于在轧制变形过程中产生的晶粒细化和加工强化.

Abstract

The effect of deformation on the microstructure and properties of semi-solid CuSnq10 alloy was investigated.Semi-solid CuSn10 slurry was made by a self-developed enclosed cooling slope channel(ECSC)and cast into thin plates by rheological squeeze,and then rolled at 350 ℃.The results show that as deformation increases,casting defects such as shrinkage porosity and shrinkage cavities gradually decrease,with grains compressed and elongated,and their average thickness is reduced from 30.58 μm(undeformed)to 22.12 μm(ε=0.4).In addition,more deformation twins are found inside the primary phase with increasing deformation.As deformation increases from 0 to 0.4,a large amount of substructures and dislocation density are introduced into the CuSn 10 alloy microstructure.At ε=0.4,textures[101],[111],and[001]are found in pole figures {110} and {111}.The mechanical properties of the plate increase,including yield strength,tensile strength,and hardness.At the deformation of 0.4,the yield strength,tensile strength and hardness reach 443 MPa,554 MPa,and 1901.2 MPa,increased by 106.1%,66.4%,and 41.6%,compared with those without deformation,respectively.But the plasticity of the plate is declined,and its elongation decreases to 0.82%.The changes in the alloy are mainly attributed to work hardening and refined grains produced during the rolling deformation.

关键词

铜锡合金/半固态/轧制变形/微观结构/EBSD

Key words

copper-tin alloy/semi-solid/rolling deformation/microstructure/EBSD

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基金项目

国家自然科学基金(51765026)

出版年

2024
稀有金属材料与工程
中国有色金属学会,中国材料研究学会,西北有色金属研究院

稀有金属材料与工程

CSTPCD北大核心
影响因子:0.634
ISSN:1002-185X
参考文献量38
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