稀有金属材料与工程2024,Vol.53Issue(4) :1075-1085.DOI:10.12442/j.issn.1002-185X.20230104

基板预热温度对选区激光熔化AlSi9Mg1ScZr微观组织及力学性能的影响

Effect of Substrate Preheating Temperature on Microstructure and Mechanical Properties of AlSi9Mg1ScZr Alloy Prepared by Selective Laser Melting

张璨 王国伟 朱京玺 王利利 沈显峰 叶寒 王超 黄姝珂
稀有金属材料与工程2024,Vol.53Issue(4) :1075-1085.DOI:10.12442/j.issn.1002-185X.20230104

基板预热温度对选区激光熔化AlSi9Mg1ScZr微观组织及力学性能的影响

Effect of Substrate Preheating Temperature on Microstructure and Mechanical Properties of AlSi9Mg1ScZr Alloy Prepared by Selective Laser Melting

张璨 1王国伟 2朱京玺 1王利利 2沈显峰 2叶寒 3王超 2黄姝珂2
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作者信息

  • 1. 中国工程物理研究院机械制造工艺研究所,四川绵阳 621900;南昌大学先进制造学院,江西南昌 330031
  • 2. 中国工程物理研究院机械制造工艺研究所,四川绵阳 621900
  • 3. 南昌大学先进制造学院,江西南昌 330031
  • 折叠

摘要

研究了基板预热温度对选区激光熔化(SLM)制备AlSi9Mg1ScZr合金样品微观组织及力学性能的影响,在35、85、135 ℃ 3种不同基板预热温度下,制备了 SLM样品并分别进行微观组织观察及性能测试.结果表明,基板预热温度设置为135 ℃时,由于基板预热温度和激光扫描热输入的共同影响,使合金在打印过程产生了原位时效效应,在保留细小枝晶和Si网格的同时促进了元素从过饱和固溶体中析出.相比基板预热35 ℃的样品,纳米尺度的Mg2Si相和Si相在α-Al基体及枝晶界析出的数量显著增加,起到了提高强度的作用;但微米尺度富Fe相的析出对塑性产生了负面影响.在基板预热温度设置为135 ℃时,制备的AlSi9Mg1ScZr合金在0°方向上屈服强度高达360 MPa、抗拉强度高达502 MPa、伸长率为7%;90°方向上屈服强度高达331 MPa、抗拉强度高达511 MPa、伸长率为5.4%.本研究通过提高基板预热温度,在SLM过程中实现了 SLM样品的原位时效,改善了 SLM制备AlSi9Mg1ScZr合金的微观组织,在不经过后续热处理的情况下,大幅降低了残余应力,得到了超高强度的AlSi9Mg1ScZr合金样品.

Abstract

The effects of substrate preheating temperature on the microstructure and mechanical properties of AlSi9MglScZr alloy samples prepared by selective laser melting(SLM)were investigated.SLM samples were prepared at three different substrate preheating temperatures of 35,85,and 135 ℃,and subjected to microstructure observation and property testing.The results show that the substrate preheating temperature set to 135 ℃ causes the in-situ aging effect of the alloy during the printing process due to the combined effect of the substrate preheating temperature and laser scanning heat input,which promotes the precipitation of elements from the supersaturated solid solution while retaining fine dendrites and Si lattices.Compared with the sample with the substrate preheated at 35 ℃,the nanoscale Mg2Si and Si phases are precipitated significantly more in the α-Al matrix and dendrite boundaries,which improves the strength;however,the precipitation of the micron-scale Fe-rich phase has a negative effect on plasticity.At a substrate preheating temperature setting of 135 ℃,the prepared AlSi9Mg1ScZr alloy exhibits a yield strength of 360 MPa,a tensile strength of 502 MPa,and an elongation of 7%in the 0° direction,and a yield strength of 331 MPa,a tensile strength of 511 MPa,and an elongation of 5.4%in the 90° direction.The microstructure of AlSi9MglScZr alloy prepared by SLM is improved by increasing the substrate preheating temperature and in-situ aging of the SLM samples is achieved during SLM,by which the residual stress is significantly reduced and ultra-high strength AlSi9Mg1ScZr alloy samples can be obtained without subsequent heat treatment.

关键词

选区激光熔化/AlSi9Mg1ScZr合金/基板预热/微观组织/力学性能

Key words

selective laser melting/AlSi9Mg1ScZr alloy/substrate preheating/microstructure/mechanical properties

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基金项目

中国工程物理研究院创新发展基金(CX20210005)

国家自然科学基金(52101057)

出版年

2024
稀有金属材料与工程
中国有色金属学会,中国材料研究学会,西北有色金属研究院

稀有金属材料与工程

CSTPCDCSCD北大核心
影响因子:0.634
ISSN:1002-185X
参考文献量28
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