首页|超高W含量NiW中/重合金热加工行为研究

超高W含量NiW中/重合金热加工行为研究

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采用Gleeble-1500D研究了 Ni-42W-10Co-1Mo(质量分数,%)中/重合金(MHA)在1150~1300 ℃和应变速率0.001~1 s-1下流变行为和微观组织演化规律.结果表明,该合金初始组织由面心立方基体和初生σ相构成.流变应力对变形温度和应变速率敏感,在较高应变速率1s-1下,应力-应变曲线呈现出典型的动态回复软化特征,而在较低应变速率0.1~0.001 s-1下变形应力-应变曲线呈现出典型动态再结晶软化特征.基于应力-应变曲线建立了 Arrhenius本构方程,并计算得到Ni-42W-10Co-1Mo合金热变形激活能为446.2 kJ/mol.基于动态材料模型构建该合金热加工图,发现在1300 ℃高应变速率下存在失稳区.通过微观组织分析,揭示其动态再结晶机制主要为不连续动态再结晶,σ相促进动态再结晶优先在其周围形核.最终优化获得了 Ni-42W-10Co-1Mo合金最佳的热加工窗口:1250~1300 ℃,应变速率0.1~0.01 s1.
Hot Workability of NiW Medium/Heavy Alloys with Ultra-high W Content
The flow behavior and microstructural evolution of a high-density Ni-42W-10Co-1Mo(wt%)alloy were investigated at 1150-1300 ℃ under strain rates of 0.001-1 s-1 using a Gleeble-1500D.The results show that the initial microstructure is composed of face-centered cubic matrix and σ phase.The flow stress is sensitive to the deformation temperature and strain rate,and the stress-strain curve shows typical dynamic revertive softening characteristics when deformed at 1 s-1,while typical dynamic recrystallization softening characteristics are observed when deformed at 0.1-0.001 s-1.The Arrhenius equation was established based on the stress-strain curves,and the hot deformation activation energy of the Ni-42W-10Co-1Mo alloy was calculated to be 446.2 kJ/mol.The thermal processing map was constructed based on the dynamic material model to evaluate the thermal processing performance,and the instable zone was located at 1300 ℃ under high strain rate.The deformation microstructural evolution reveals that the dynamic recrystallization mechanism is discontinuous dynamic recrystallization,which preferentially nucleates around the σ phase.Finally,the optimized hot working window for Ni-42W-10Co-1Mo alloy was obtained at 1250-1300 ℃ under strain rate of 0.1-0.01 s-1.

MHAnickel-based alloythermal processingconstitutive relationship

曹国鑫、董建新、张胜、姚志浩、解国良、聂志华、马腾飞、付宝全

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北京科技大学材料科学与工程学院,北京 100083

西安聚能高温合金材料科技有限公司,陕西西安 710299

北京理工大学材料学院,北京 100081

衢州学院浙江省空气动力装备技术重点实验室,浙江衢州 324000

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中重合金 镍基合金 热加工 本构关系

国家自然科学基金

51771016

2024

稀有金属材料与工程
中国有色金属学会,中国材料研究学会,西北有色金属研究院

稀有金属材料与工程

CSTPCD北大核心
影响因子:0.634
ISSN:1002-185X
年,卷(期):2024.53(5)
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