首页|超细晶挤压态FGH4113A高温合金等温锻造过程中的本构特性及组织演变

超细晶挤压态FGH4113A高温合金等温锻造过程中的本构特性及组织演变

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锻造是先进航空发动机粉末涡轮盘制备的关键成型工艺.合金的化学成分和挤压工艺很大程度上决定了挤压态合金的组织.新型镍基粉末高温合金FGH4113A(WZ-A3)热挤压之后晶粒度达到13级以上,挤压态合金呈现γ+γ'双相组织.细小均匀的双相组织为更为广阔的等温锻造工艺窗口提供可能.本研究采用超细晶挤压态合金FGH4113A进行温度分别为1000、1040、1080和1120 ℃,应变速率为0.001、0.01和0.1 s-1的Gleeble热压缩试验,压缩量为60%.结果表明合金试样在所有压缩条件下均未发生开裂,体现超细晶挤压态合金FGH4113A有广阔的等温锻造工艺窗口.合金的平均激活能仅为515.375 kJ/mol.低应变速率下(0.001 s-1),试样真应力-真应变曲线呈现出稳态流变特性;高应变速率下(0.1s-1),试样的真应力-真应变曲线呈现出加工硬化到再结晶软化的变化.γ'相对变形温度敏感,高的变形温度会引发γ'相的溶解而导致再结晶晶粒的长大.此外,超细晶挤压态合金FGH4113A在等温锻造过程中主要再结晶方式为不连续动态再结晶.本研究为超细晶挤压态合金FGH4113A的锻造工艺制定提供了实验依据.
Constitutive Characterization and Microstructure Evolution of As-extruded FGH4113A Superalloy with Ultrafine Grain During Isothermal Forging
Forging is the key forming process for producing advanced aero-engine powder turbine disks.The microstructure of as-extruded alloy mostly depends on the chemical composition of alloy and extrusion processing parameters.The average grain size number is greater than 13 for the novel powder nickel-based superalloy FGH4113A after hot extrusion,and the as-extruded alloy has dual-phase microstructure of γ+γ'.The fine and homogeneous dual-phase microstructure makes it possible to broaden isothermal forging processing window.In this study,Gleeble hot compression experiments for as-extruded FGH4113A alloy with ultrafine grains were carried out at temperatures of 1000,1040,1080,1120 ℃ and strain rates of 0.001,0.01,0.1 s-1.Height reduction was 60%for samples under all experiment conditions.The results show that no crack is found on the surface of alloy samples under all experiment conditions,suggesting that the as-extruded FGH4113A alloy with ultrafine grains has a wide isothermal forging process window.The average activation energy for the alloy is 515.375 kJ/mol.True stress-true strain curves show a steady flow characteristic for samples under low strain rate(0.001 s-1)and the change from work hardening to recrystallization softening for the samples under high strain rate(0.1 s-1).γ'is sensitive to temperature,and recrystallization grains grow obviously at high deformation temperature due to the dissolution of a large amount of γ'.Furthermore,the main recrystallization way is discontinuous dynamic recrystallization for as-extruded FGH4113A alloy with ultrafine grains.This study offers experiment evidence for forging processing design of the as-extruded FGH4113A alloy with ultrafine grains.

ultrafine grainhot extrusionFGH4113Aisothermal forgingmicrostructure evolution

李远、何英杰、马向东、杨金龙、肖磊、郭建政、冯干江

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深圳市万泽中南研究院有限公司,广东深圳 518000

深圳市万泽航空科技有限责任公司,广东深圳 518000

中南大学粉末冶金研究院,湖南长沙 410083

超细晶 热挤压 FGH4113A 高温锻造 组织演变

国家科技重大专项深圳市工业和信息化局项目深圳市科技创新委员会项目广东省珠江人才计划

2017-Ⅵ-0009-008020180607111424377020150128085205453607264877417

2024

稀有金属材料与工程
中国有色金属学会,中国材料研究学会,西北有色金属研究院

稀有金属材料与工程

CSTPCD北大核心
影响因子:0.634
ISSN:1002-185X
年,卷(期):2024.53(8)