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冷热循环处理对热等静压铍材尺寸稳定性的影响

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利用激光测长仪、拉曼光谱仪、纳米压痕仪、背散射衍射电镜以及透射电镜分析不同处理状态等静压铍材的尺寸变化、残余应力、晶粒取向差、位错密度及位错分布形态,分析冷热循环处理对铍材尺寸稳定性的影响.结果表明,热等静压铍材在-100~150 ℃冷热循环6次后尺寸趋于稳定,具有良好的尺寸稳定性.冷热循环处理过程中铍材尺寸稳定化机制主要是晶粒内位错均匀化及微塑性变形导致取向差均匀化.
Effects of Thermal-Cold Cycling on Dimensional Stability of HIPed Beryllium
The dimensional change,residual stress,grain orientation difference,dislocation density,and dislocation distribution of beryllium after different hot isostatic pressing treatments were analyzed by laser length meter,Raman spectrometer,nanoindentation meter,electron backscattered diffractometer,and transmission electron microscope,and the influence of thermal-cold cycling treatment on the dimensional stability of beryllium was analyzed.Results show that the size of the hot isostatic pressed beryllium tends to be stable after 6 cycles of thermal-cold cycling treatment from-100 ℃ to 150 ℃,and it has good dimensional stability.The dimensional stabilization mechanism of beryllium is mainly the homogenization of dislocations within the grain and the homogenization of orientation difference caused by micro-plastic deformation.

berylliumthermal-cold cyclingmicrostructuredimensional stability

任鹏禾、肖来荣、蔡圳阳、涂晓萱、赵小军

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中南大学材料科学与工程学院,湖南长沙 410083

有色金属材料科学与工程教育部重点实验室,湖南长沙 410083

铍材 冷热循环处理 组织结构 尺寸稳定性

National Defense Basic Scientific Research Program of ChinaYouth Natural Science Foundation of Hunan Province

JCKY2018203B0672019JJ50817

2024

稀有金属材料与工程
中国有色金属学会,中国材料研究学会,西北有色金属研究院

稀有金属材料与工程

CSTPCD北大核心
影响因子:0.634
ISSN:1002-185X
年,卷(期):2024.53(10)