压电与声光2024,Vol.46Issue(4) :545-549.DOI:10.11977/j.issn.1004-2474.2024.04.021

钽酸锂单晶薄膜的退火处理与微结构分析

Study of Thermal Annealing and Microstructure Analysis on Crystal-Ion-Sliced LiTaO3 Single Crystal Thin Film

杨杰 高艺卓 朱代磊 帅垚 吴传贵 罗文博
压电与声光2024,Vol.46Issue(4) :545-549.DOI:10.11977/j.issn.1004-2474.2024.04.021

钽酸锂单晶薄膜的退火处理与微结构分析

Study of Thermal Annealing and Microstructure Analysis on Crystal-Ion-Sliced LiTaO3 Single Crystal Thin Film

杨杰 1高艺卓 1朱代磊 1帅垚 2吴传贵 2罗文博2
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作者信息

  • 1. 电子科技大学 集成电路科学与工程学院,四川 成都 611731
  • 2. 电子科技大学 集成电路科学与工程学院,四川 成都 611731;电子科技大学 电子薄膜与集成器件国家重点实验室,四川 成都 611731
  • 折叠

摘要

离子注入剥离技术制备的钽酸锂单晶薄膜可用于高品质因数和低热漂移窄带射频滤波器,但高能离子注入使钽酸锂薄膜存在缺陷及晶格损伤,限制了器件性能的提升,无法充分发挥单晶薄膜的性能优势.使用退火工艺对钽酸锂薄膜进行损伤修复,采用拉曼光谱对不同温度退火的钽酸锂薄膜进行表征测试,分析了退火温度对钽酸锂薄膜成分和缺陷的影响.结果表明,退火处理修复了钽酸锂薄膜的锂空位缺陷,降低了钽酸锂薄膜的氧空位等成分偏析.

Abstract

Lithium tantalate(LiTaO3)single-crystal thin films are utilized for high-Q and low thermal drift nar-row-band RF filters based on crystal ion slicing(CIS)technology.However,defects and lattice damage caused by high-energy ion implantation in LiTaO3 films hinder the enhancement of device performance.In this study,we em-ployed a thermal annealing process to repair the damage in LiTaO3 films and characterize the defects using Raman spectroscopy.Additionally,we analyzed the impact of annealing temperature on the composition and defects of LiTaO3 films.The results demonstrate that thermal annealing effectively repairs lithium vacancy defects and reduces oxygen vacancies in LiTaO3 films.

关键词

钽酸锂单晶薄膜/退火处理/拉曼光谱/晶体缺陷/薄膜成分偏析

Key words

lithium tantalate single-crystal film/thermal annealing treatment/Raman spectroscopy/lattice damage/film composition segregation

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出版年

2024
压电与声光
四川压电与声光技术研究所

压电与声光

CSTPCD北大核心
影响因子:0.357
ISSN:1004-2474
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