首页|全自动消解-原子荧光法测定管网水中硒和砷

全自动消解-原子荧光法测定管网水中硒和砷

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建立了全自动湿法消解-氢化物发生原子荧光光谱法同时对水中痕量硒(Se)和砷(As)元素进行分析测定的方法.标准曲线线性关系良好(r≥0.9995),方法加标回收率(n=6)为 89.0%~104.2%,RSD 值(n=6)为 1.3%~6.4%,方法检出限分别为 0.048µg/L及 0.051µg/L.该法具有操作简单和高效分析的优点,并成功用于大批量水中硒和砷的同时定量分析.
Determination of Trace Amounts of Selenium in Water by Automatic Wet Digestion-Atomic Fluorescence Spectrometry
Trace amounts of selenium and arsenic in water were determined by Automatic wet digestion-atomic Fluorescence spectrometry.The linear correlations of standard curves were good(r≥0.9995).The recovery rate was in the range of 89.0%to 104.2%(n=6),and the relative standard deviation(RSD)of this method was(n=6)between 1.3%and 6.4%.The detection limit of selenium and arsenic were 0.048µg/L and 0.051µg/L.This method has the advantages of simple operation and efficient analysis,and were successfully used for the determination of selenium and arsenic in quantities of water.

automatic wet digestionatomic fluorescencewaterselenium arsenic

雷红琴、牛鸣光、尚爽、徐颖洁、粟有志、李芳、李艳美、王兴磊

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伊犁师范大学化学与环境科学学院 污染物化学与环境治理重点实验室,新疆 伊宁 835000

伊宁海关技术中心,新疆 伊宁 835000

喀什海关技术中心,新疆 喀什 844000

全自动湿法消解 原子荧光 管网水

伊犁师范大学污染物化学与环境伊犁师范大学污染物化学与环境治理重点实验室开放基金

2021HJYB03

2024

饮料工业
中国饮料工业协会

饮料工业

影响因子:0.315
ISSN:1007-7871
年,卷(期):2024.27(1)
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