首页|基于特征成分的料香均匀性方法建立及评价

基于特征成分的料香均匀性方法建立及评价

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以云产某品牌规格加料及加香叶组烟丝为对象,采用Weight Analysis和SR 变量筛选方法对料、香叶组烟丝的挥发性成分进行特征筛选,筛选出棕榈酸甲酯、亚麻酸乙酯和二十四烷3 个料香中的特征物质,并与传统标记物丙二醇、薄荷醇进行料香均匀性对比评价.结果显示:①在含量分布上,亚麻酸乙酯、丙二醇在表香中含量分布较高,二十四烷在料液中含量分布较高,具有极其显著统计学意义.薄荷醇在料液中含量较高,具有统计学意义.棕榈酸甲酯在表香样品中含量分布稍高,无统计学意义;②在区分能力上,5 个物质对加料和加香样本区分能力各不相同,从强至弱分别是二十四烷(100%)、亚麻酸乙酯(98.15%)、丙二醇(83.30%)、薄荷醇(65.74%)和棕榈酸甲酯(52.78%),所筛选二十四烷和亚麻酸乙酯可作为料香的标记物;③从料香均匀性评价效果上,亚麻酸乙酯和二十四烷评价结果一致,均表现为滚筒干燥工序料香均匀性最高,加料阶段其次,加香阶段最差,与实际认知相同.薄荷醇和丙二醇二者评价结果出现差异;④从评价结果相似度上看,亚麻酸乙酯和二十四烷对加料、滚筒干燥和加香工序的均匀性评价结果极为吻合,亚麻酸乙酯特征标记物三阶段评价结果分别为92.01%、92.19%和88.76%,采用二十四烷评价结果分别为 93.44%、93.93%和 86.64%,二者评价结果相似性达0.999,而薄荷醇和丙二醇的评价相似度仅有0.136.
Establishment and Application of Tobacco Blending Uniformity Evaluation Method Based on Chemical Composition
The weight analysis and SR variable screening methods were used to screen the volatile components of the cut tobacco of a brand in Yunnan.The characteristic substances of methyl palmitate,ethyl linolenic acid and tetracosane were screened out and compared with the tradi-tional markers of propylene glycol and menthol.The results showed that:(1)In terms of content distribution,ethyl linolenate and propylene gly-col have a higher content distribution in the tobacco flavor,and tetracosane has a higher content distribution in the tobacco casing,which has ex-tremely significant statistical significance.The content of menthol in the tobacco casing with high level has significance in statistics.The distribu-tion of methyl palmitate in the tobacco flavor samples is slightly higher,which is not statistically significant.(2)In discrimination ability,five substances have shown different ability in distinguishing between cased and flavored samples.From strong to weak:tetracosane(100%),ethyl linolenate(98.15%),propylene glycol(83.30%),and menthol(65.74%).)and methyl palmitate(52.78%).The selected tetracosane and ethyl linolenate can be used as markers for flavor fragrance.(3)In terms of the effect of uniformity,the results of the evaluation of ethyl linole-nate and tetracosane are consistent.Both showed that the uniformity of the flavor in the drum drying process is the highest,followed by the feed-ing stage,and the worst in the flavoring stage,which is the same as actual knowledge.The evaluation results of menthol and propylene glycol are different.(4)According to the similarity of the evaluation results,the uniformity evaluation results of ethyl linolenate and tetracosane on the feed-ing,drum drying and flavoring process are very consistent.The three-stage evaluation results of the ethyl linolenate are 92.01%,92.19%and 88.76%,the evaluation results of tetracosane were 93.44%,93.93%and 86.64%,respectively.The similarity for two characteristic marker of the evaluation results was 0.999,while the menthol and propylene glycol was only 0.136.

uniformity of flavoringvariable selectioncharacteristic componentsmarkers

杨乾栩、赵蔚、谢志强、杨洪明、李超、刘欣、张伟

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云南中烟工业有限责任公司 技术中心, 云南 昆明 650231

料香均匀性 变量筛选 特征成分 标记物

云南中烟工业有限责任公司科技项目云南中烟工业有限责任公司科技项目

2022HX012021YL02

2024

云南化工
云南省化工研究院 云天化集团有限责任公司 云南煤化工集团有限公司 云南省化学化工学会

云南化工

影响因子:0.272
ISSN:1004-275X
年,卷(期):2024.51(2)
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