首页|ICP-OES有机直接进样法测定食品添加剂中铁、钙、铝、铅、锌、砷

ICP-OES有机直接进样法测定食品添加剂中铁、钙、铝、铅、锌、砷

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建立了ICP-OES(电感耦合等离子体发射光谱仪)有机直接进样测定复配食品添加剂中铁、钙、铝、铅、锌、砷共6种元素含量的方法.采用乙醇溶液为稀释剂,按一定比例稀释后直接进仪器检测.结果表明,这6种元素在0.05~5.00 mg/L线性关系良好,相关系数均大于0.9999,检出限为0.0001~0.0016mg/L,加标回收率为91.4%~108.4%,相对标准偏差为0.53%~3.65%.该方法操作简单,准确度高,安全快捷,可用于复配食品添加剂中的杂质元素检测.
Determination of Iron,Calcium,Aluminum,Lead,Zinc and Arsenic in Food Additives by Directly Introduction under Method of Organic Phase Using ICP-OES
Inductively Coupled Plasma Optical Emission Spectrometer(ICP-OES)was proposed to determine of 6 elements including iron,calci-um,aluminum,lead,zinc and arsenic in food additives by directly introduction under method of organic phase.With ethanol solution as a diluent,the samples are directly analyzed after being diluted according to a specific ratio,the results showed that good linearity in the concentration range of 0.05-5.00 mg/L and the correlation coefficient was over 0.9999,the limits of detection(LODs)of all the elements were in the range from 0.0001-0.0016 mg/L,the average recoveries were 91.4%-108.4%,and the relative standard deviations(RSD)were 0.53%-3.65%.This method is simple to operate,highly accurate,safe and fast.It can be used for detecting impurity elements in compound food additives.

ICP-OESMethod of Organic Phase SamplingFood AdditivesImpurity Elements

荣沙沙、杜建侠、李红、肖清燕、卢会珍

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湖北三峡实验室,湖北 宜昌 443000

ICP-OES 有机进样法 食品添加剂 杂质元素

2024

云南化工
云南省化工研究院 云天化集团有限责任公司 云南煤化工集团有限公司 云南省化学化工学会

云南化工

影响因子:0.272
ISSN:1004-275X
年,卷(期):2024.51(4)
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