云南化工2024,Vol.51Issue(9) :93-95.DOI:10.3969/j.issn.1004-275X.2024.09.20

湿法消解-石墨炉原子吸收光谱法测定花椒中的铅

Determination of Lead Content in Zanthoxylum bungeanum by Wet Digestion-Graphite Furnace Atomic Absorption Spectroscopy

刘强 牟春燕 黄礼丽
云南化工2024,Vol.51Issue(9) :93-95.DOI:10.3969/j.issn.1004-275X.2024.09.20

湿法消解-石墨炉原子吸收光谱法测定花椒中的铅

Determination of Lead Content in Zanthoxylum bungeanum by Wet Digestion-Graphite Furnace Atomic Absorption Spectroscopy

刘强 1牟春燕 2黄礼丽1
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作者信息

  • 1. 四川化工职业技术学院,四川 泸州 646300
  • 2. 泸州市林业科学研究院,四川 泸州 646099
  • 折叠

摘要

花椒是云、贵、川、渝等地区餐桌上的常用调料.花椒中重金属的含量直接影响人们的身体健康,其质量安全检验监测尤为重要.采用湿法消解-石墨炉原子吸收光谱法测定花椒中的Pb含量.在最佳仪器条件下,对四川省内江市不同地区的25个花椒样品进行了测定,方法的线性范围为0.00~200.00 ng/mL,检出限为0.005 mg/L.方法的精密度良好,相对极差为9.93%;方法准确,质控样品测定结果的相对误差为-7.50%~-16.25%.25个花椒样品的Pb含量均未超过GB 2762-2022食品中污染物限量所规定的限量标准.

Abstract

Zanthoxylum bungeanum is a commonly used seasoning on dining tables in regions such as Yunnan,Guizhou,Sichuan,and Chongqing.The content of heavy metals in Zanthoxylum bungeanum directly affects people's physical health,and its quality and safety inspec-tion and monitoring are particularly important.This article uses wet digestion-graphite furnace atomic absorption spectroscopy to determine the Pb content in Zanthoxylum bungeanum.Under optimal instrument conditions,25 Zanthoxylum bungeanum samples from different regions in Si-chuan Provice were measured,with a linear range of 0.00-200.00 ng/mL and a detection limit of 0.005 mg/L.The precision of the method is good,with a relative range of 9.93%;The method is accurate,and the relative error of the quality control sample determination results is-7.50%--16.25%.The Pb content of Zanthoxylum bungeanum samples from 25 different regions has not exceeded the limit standard for pol-lutants in food specified in GB 2762-2022.

关键词

/花椒/石墨炉原子吸收光谱法/湿法消解

Key words

Lead/Zanthoxylum Bungeanum/GF-AAS/Wet Digestion

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出版年

2024
云南化工
云南省化工研究院 云天化集团有限责任公司 云南煤化工集团有限公司 云南省化学化工学会

云南化工

影响因子:0.272
ISSN:1004-275X
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