云南化工2024,Vol.51Issue(z1) :25-28.DOI:10.3969/j.issn.1004-275X.2024.Supp.05

探讨ICP法快速测定磷酸中Fe、Al、Mg的质量分数

Exploring the Rapid Determination of Fe,Al,Mg Mass Fractions in Phosphoric Acid by ICP Method

杨昌洲
云南化工2024,Vol.51Issue(z1) :25-28.DOI:10.3969/j.issn.1004-275X.2024.Supp.05

探讨ICP法快速测定磷酸中Fe、Al、Mg的质量分数

Exploring the Rapid Determination of Fe,Al,Mg Mass Fractions in Phosphoric Acid by ICP Method

杨昌洲1
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作者信息

  • 1. 云南天安化工有限公司生产技术部,云南 安宁 650309
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摘要

磷酸中铁、铝、镁含量直接影响磷肥产品的质量.Fe、Al、Mg含量偏高时,会导致产品发干发枯.电感耦合等离子发射光谱法,可快速测定磷酸中Fe、Al、Mg的质量分数,加标回收率在95%~105%之间,符合测定要求.该法操作快速、简便,可替代化学滴定法.

Abstract

The content of iron,aluminum,and magnesium in phosphate directly affects the quality of phosphate fertilizer products.When the content of Fe,Al,and Mg is too high,it can cause the product to dry and wither.Therefore,exploring the use of inductively coupled plasma e-mission spectroscopy for rapid determination of Fe,Al,and Mg mass fractions in phosphoric acid,with a spiked recovery rate between 95%and 105%,meets the measurement requirements.This method is fast and simple to operate,and can replace chemical titration.

关键词

ICP快速测定/磷酸//

Key words

ICP Rapid Determination/Phosphoric Acid/Iron/Aluminium

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出版年

2024
云南化工
云南省化工研究院 云天化集团有限责任公司 云南煤化工集团有限公司 云南省化学化工学会

云南化工

影响因子:0.272
ISSN:1004-275X
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