首页|GC-MS法分析不同品牌藏香产品的化学成分

GC-MS法分析不同品牌藏香产品的化学成分

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为分析名优品牌藏香产品的化学成分及特征物质信息,以正己烷-丙酮混合溶液作为提取溶剂,对藏香样品进行超声提取,所得提取液经过滤后,再进样至气相色谱-质谱联用仪中分析并鉴定化学成分,通过峰面积归一化法获得各化合物相对百分含量.结果表明,从A品牌藏香、B品牌藏香和C品牌藏香样品中分别鉴定出 61、62 和 34 种化合物,其中包括 16 种共有成分:雪松醇、异土木香内酯、土木香内酯、去氢木香内酯、表木栓醇、丁香酚、β-香树脂醇、24-norursa-3,12-dien-11-one、24-norursa-3,12-diene、无羁萜、α-香树脂醇、熊果醛、24-noroleana-3,12-diene、日柏酮、桉油烯醇、正二十九烷,上述共有成分平均相对含量依次为4.36%、4.35%、3.68%、3.19%、2.63%、2.43%、1.75%、1.53%、1.45%、1.31%、1.26%、0.90%、0.81%、0.59%、0.40%、0.33%,其中雪松醇是藏香样品中平均含量最高的化合物.另外,这些共有成分中有 14 种为萜类,且在上述 3 种样品中萜类总量占共有成分比例分别为93.29%、93.93%、86.66%,表明萜类成分是藏香共有成分中数量最多、相对含量占比最大的一类化合物.综上,通过GC-MS法获得藏香产品化学成分及其特征成分,可为后续藏香产品的进一步研究和开发提供科学依据和参考.
GC-MS analysis of chemical constituents of Tibetan incense products from different brands
In order to analyze the chemical composition and characteristic substance information of famous and ex-cellent brand Tibetan incense products,the filtrate of Tibetan incense samples extracted by ultrasonic with n-hex-ane acetone mixture was analyzed by gas chromatography-mass spectrometry(GC-MS).The chemical compo-nents of the extract of Tibetan incense products were analyzed and identified.The relative percentage content of each compound was obtained by peak area normalization method.The results showed that 61,62 and 34 com-pounds were identified from the three samples of Tibetan incense sample A,Tibetan incense sample B,and Tibetan incense sample C,including 16 co-constituents:cedrol,isoalantolactone,alantolactone,dehydrocostus lactone,epifriedelinol,eugenol,β-amyrin,24-norursa-3,12-dien-11-one,24-norursa-3,12-diene,friede-lan-3-one,α-amyrin,ursolic aldehyde,24-noroleana-3,12-diene,hinokione,(-)-spathulenol,non-acosane,The average relative contents of the above common components were 4.36%,4.35%,3.68%,3.19%,2.63%,2.43%,1.75%,1.53%,1.45%,1.31%,1.26%,0.90%,0.81%,0.59%,0.40%and 0.33%respectively.Cedrol was the compound with the highest average content in Tibetan incense samples.In addition,14 of these common components were terpenes,and the total terpenes in the above three samples accounted for 93.29%,93.93%and 86.66%of the common components,respectively,indicating that the terpenoids were the most numerous and the largest proportion of the relative content of the common components of Tibetan incense.In conclusion,the chemical components and characteristic components of Tibetan incense products obtained by GC-MS can provide scientific basis and reference for further research and development of Tibetan incense products.

Tibetan incenseincense productGC-MScomponent analysis

涂永元

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国家燃香类产品质量检验检测中心(福建),福建 永春 362600

永春县产品质量检验所,福建 永春 362600

福建省香产品质量检验中心,福建 永春 362600

藏香 燃香产品 GC-MS 成分分析

福建省市场监督管理局科技计划项目福建省引导性科技计划项目

FJMS20220462023Y6002

2024

云南民族大学学报(自然科学版)
云南民族大学

云南民族大学学报(自然科学版)

CSTPCD
影响因子:0.381
ISSN:1672-8513
年,卷(期):2024.33(5)
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