首页|以β-CD为模板剂制备Pr-TiO2纳米催化剂及其光催化降解性能

以β-CD为模板剂制备Pr-TiO2纳米催化剂及其光催化降解性能

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采用β-环糊精(β-CD)为模板剂,利用溶胶-凝胶法制备了TiO2、Pr-TiO2纳米催化剂,通过X射线衍射(XRD)、扫描电镜(SEM)、傅立叶红外光谱(FT-IR)和N2吸附-脱附等技术对所制备的催化剂进行了表征,优化了纳米催化剂的制备条件,并分别在紫外光和可见光照下以降解含罗丹明B(RhB)的印染废水评价其光催化降解性能.结果表明,以β-CD为模板剂制备的纳米复合催化剂粒径更小,Pr-TiO2在紫外、可见光下的脱色率分别达92%和97%以上,较TiO2催化剂的性能有所提高.
Preparation of Pr-TiO2 nanocomposite catalyst using β-CD as template and its photocatalytic activity
Nanocomposite catalysts of TiO2 and Pr-TiO2 was prepared by sol-gel method using β-cyclo-dextrin (β-CD) as template.X-ray diffraction (XRD),scanning electron microscopy (SEM),Fourier transform infrared spectroscopy (FT-IR) and N2 adsorption-desorption were used for catalyst characterization.And the preparation conditions of nanocomposite catalyst were investigated.The photocatalytic activities of prepared nanocomposites were investigated by the degradation of Rhodamine B (RhB) dye wastewater under the illumination of UV and visible light,respectively.The results showed that the particle size of nanocomposite catalyst with β-CD template was smaller,and the decoloration rate of Pr-TiO2 nanocomposite formed by the above method was more than 92% and 97% under UV and visible light irradiation,respectively.Compared with the photocatalytic performance of TiO2,they exhibited high activity.

titanium dioxidephotocatalyticβ-CDdegradation

贾帅强、隋国哲、李金龙、佟白

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齐齐哈尔大学化学与化学工程学院,黑龙江齐齐哈尔161006

二氧化钛 光催化 β-CD 降解

黑龙江省科学基金资助项目

LC2011C36

2016

印染助剂
江苏苏豪传媒有限公司

印染助剂

CSTPCD北大核心
影响因子:0.476
ISSN:1004-0439
年,卷(期):2016.33(10)
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