首页|CVD Al2O3涂层织构取向对显微组织结构和性能的影响

CVD Al2O3涂层织构取向对显微组织结构和性能的影响

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化学气相沉积(CVD)Al2O3涂层具备高硬度,良好韧性,优异的耐磨、耐热、抗氧化、化学稳定等性能,是一种综合性能优良的切削刀具涂层材料。本文采用CVD制备了具有(104)、(0012)及(012)织构取向α-Al2O3的MT-TiCN/Al2O3/TiN涂层。采用XRD、SEM等研究了涂层显微组织结构、织构取向及涂层性能。实验结果表明,高(0012)织构取向α-Al2O3涂层柱状晶晶粒更完整;α-Al2O3涂层织构取向会影响表层TiN形貌及织构取向,高(0012)织构取向α-Al2O3表层TiN为高(111)织构取向,(104)织构取向α-Al2O3表层TiN为弱(111)+(331)混合织构取向,(012)织构取向α-Al2O3表层TiN为弱(220)+(420)混合织构取向。车削42CrMo实验结果表明,高(0012)织构取向α-Al2O3涂层耐磨性能优于(104)和(012)织构取向,主要表现在高(0012)织构取向α-Al2O3涂层前刀面和后刀面抗磨损能力均更优。
Influence of Texture Orientation of CVD Al2O3 Coating on Microstructure and Properties
The chemical vapor deposition(CVD)Al2O3 coating possesses high hardness,good toughness,as well as excellent wear resistance,heat resistance,oxidation resistance,and chemical stability.It is a cutting tool coating material with excellent comprehensive properties.In this paper,the MT-TiCN/Al2O3/TiN coatings with(104),(0012),and(012)texture orientations of α-Al2O3 were prepared by CVD.The microstructures,texture orientations,and coating properties were studied by using X-ray diffraction(XRD)and scanning electron microscope(SEM).The experimental results show that the columnar grains of the α-Al2O3 coating with high(0012)texture orientation are more complete.The texture orientation of the α-Al2O3 coating will affect the morphology and texture orientation of the surface TiN.The surface TiN of the α-Al2O3 coating with a high(0012)texture orientation exhibits a high(111)texture orientation.The surface TiN of the α-Al2O3 coating with a(104)texture orientation shows a weak(111)+(331)mixed texture orientation.The surface TiN of the α-Al2O3 coating with a(012)texture orientation presents a weak(220)+(420)mixed texture orientation.The results of the cutting experiment on 42CrMo indicate that the wear resistance of the α-Al2O3 coating with a high(0012)texture orientation is superior to that of the coatings with(104)and(012)texture orientations,mainly manifested in that both the rake face and the flank face of the α-Al2O3 coating with a high(0012)texture orientation have better wear resistance.

CVD coatingα-Al2O3texture orientationmicrostructurecutting performance

瞿峻、陈响明、王社权、温光华、刘萍、罗学全、李思敏

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株洲钻石切削刀具股份有限公司,湖南 株洲 412000

硬质合金国家重点实验室,湖南 株洲 412000

CVD涂层 α-Al2O3 织构取向 显微组织 切削性能

2024

硬质合金
株洲硬质合金集团有限公司

硬质合金

CSTPCD
影响因子:0.754
ISSN:1003-7292
年,卷(期):2024.41(6)