超硬材料工程2024,Vol.36Issue(6) :40-44.

金刚石微粉强度测试方法

Strength Test Approach of Diamond Micropowder

权乐 杨希 叶中郎 田芳 甄桓 信石玉 全兵 叶道辉
超硬材料工程2024,Vol.36Issue(6) :40-44.

金刚石微粉强度测试方法

Strength Test Approach of Diamond Micropowder

权乐 1杨希 1叶中郎 1田芳 1甄桓 1信石玉 1全兵 1叶道辉1
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作者信息

  • 1. 中石化江钻石油机械有限公司,湖北武汉 430223;中石化石油机械股份有限公司,湖北武汉 430223
  • 折叠

摘要

近几十年来,我国在人造金刚石单晶和金刚石微粉的研发和生产上进展迅速,已经成为世界人造金刚石单晶和金刚石微粉生产大国,世界50%以上的人造金刚石制品来自于中国.目前金刚石单晶的评价手段较为完善,不管是单晶强度、杂质含量、粒径还是形貌等均具有成熟通用的表征方法.现在市场上多以中南钻石的金刚石单晶为参照标准,根据其强度将金刚石单晶分为1~9型.但是金刚石单晶破碎料即金刚石微粉的评价手段仍有所欠缺,尤其是金刚石微粉的强度测试方法至今仍没有市场普遍认可的表征方法.如今,金刚石微粉的强度测试方法有拉曼光谱法、红外光谱法、冲击韧性法和冷压破碎法等.文章研究对比了几种测试方法的特点,并重点介绍了拉曼光谱法测试微粉强度的案例.

Abstract

In recent decades,China has made rapid progress in the research and production of single crystal diamond and diamond micropowder,and has become the world's largest producer of single crystal diamond and diamond micropowder.More than 50%of the world's synthetic diamond products come from China.Currently the single crystal diamond from ZhongNan Diamond Co.,LTD is used as reference standard in the market,and is di-vided into 1~9 types according to its strength.At present,there are mature and universal characterization methods for single crystal strength,impurity content,particle size and morphology.The evaluation methods of single crystal diamond are relatively all-sided.However,there is a short of evaluation methods for single crystal diamond crushed mi-cropowder,especially the strength test method of diamond powder is still not the charac-terization method generally recognized by the market.Nowadays,the strength test meth-ods of diamond micropowder include Raman spectroscopy,infrared spectroscopy,impact toughness method and cold press crushing method.In this paper,the characteristics of four testing methods are studied and compared,and the Raman spectroscopy testing and analyzing method is introduced in detail.

关键词

金刚石单晶/金刚石微粉/强度/拉曼光谱/冲击韧性

Key words

single crystal diamond/diamond micropowder/strength/raman spectrum/impact toughness

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出版年

2024
超硬材料工程
桂林矿产地质研究院

超硬材料工程

影响因子:0.201
ISSN:1673-1433
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