首页|基于机器人和流水线技术的高锰酸盐指数全自动分析系统研究

基于机器人和流水线技术的高锰酸盐指数全自动分析系统研究

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应用 2 套全流程自动操作的分析系统对水质高锰酸盐指数进行测定.当样品取样量为 100 mL时,2 套系统的酸性法检出限分别为 0.05 mg/L和 0.08 mg/L,标准样品的相对标准偏差在 0.86%~2.7%之间,相对误差在 1.2%~7.8%之间,实际水样的相对标准偏差在 0%~8.0%之间;碱性法的检出限分别为 0.10 mg/L和 0.06 mg/L,标准样品的相对标准偏差在 0.66%~5.2%之间,相对误差在 0.25%~11%.自动分析方法与传统手工滴定结果无显著差异,且各方法学指标优于传统方法.基于机器人和流水线技术的高锰酸盐指数全自动分析系统通过相应模块完成自动进样、自动稀释、自动传送、自动清洗等功能,利用全流程视频监控水样颜色变化过程并精准确定终点,提高了分析结果的准确度和精密度,同时全程留痕,进一步加强了质控措施,在化学分析和在环境监测实际应用中具有广阔前景.
Research on Automatic Permanganate Index Analysis System Based on Robotics and Pipeline Technology
In this paper,the permanganate index of water quality was determined by two sets of automatic analysis systems.When the sample volume is 100 mL,the detection limits of the acid method of the two systems are 0.05 mg/L and 0.08 mg/L respectively,the relative standard deviation of the standard sample is 0.86%~2.7%,the relative error is 1.2%~7.8%,and the relative standard deviation of the actual water sample is 0%~8.0%.The detection limits of the alkaline method are 0.10 mg/L and 0.06 mg/L,respectively.The relative standard deviation of the standard sample is 0.66%~5.2%,and the relative error is 0.25%~11%.Compared with the traditional manual titration,the automatic analysis method has no significant difference,and the methodological indicators are better than the traditional method.The fully automatic permanganate index analysis system based on robot and pipeline technology completes the functions of automatic sample injection,automatic dilution,automatic transmission and automatic cleaning,etc.through the corresponding modules.It uses the whole process video to monitor the color change process of the water sample and accurately determine the end point,improving the accuracy and precision of the analysis results,while leaving traces throughout the process,further strengthening the quality control measures,and has broad prospects in chemical analysis and practical application of environmental monitoring.

robotspipeline technologypermanganate indexfully automated analysis systemsenvironmental monitoring

汪凌佳、王奕奕、俞雅雲、陈峰、王立群、张明

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浙江省杭州生态环境监测中心,浙江杭州 310012

机器人 流水线技术 高锰酸盐指数 全自动分析系统 环境监测

&&杭州市科技计划引导项目

20201203B14620191231Y065

2024

自动化应用
重庆西南信息有限公司

自动化应用

影响因子:0.156
ISSN:1674-778X
年,卷(期):2024.65(7)
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