中国保健营养(上旬刊)2014,Issue(1) :42-42.DOI:10.3969/j.issn.1004-7484(s).2014.01.040

应用热分析法鉴别不同产地的丹参及其提取物

Application of Thermal Analysis in Salvia Miltiorrhiza and its Extracts from Different Origin

巩峰
中国保健营养(上旬刊)2014,Issue(1) :42-42.DOI:10.3969/j.issn.1004-7484(s).2014.01.040

应用热分析法鉴别不同产地的丹参及其提取物

Application of Thermal Analysis in Salvia Miltiorrhiza and its Extracts from Different Origin

巩峰1
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作者信息

  • 1. 山东省平邑县人民医院药剂科,山东 平邑 273300
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摘要

目的:对不同产地的两种丹参用差示扫描量热( DSC)法进行分析鉴别,鉴别内容包括:原药材粉末、水提物和醇提物。方法以α-Al2 O3作为对比参比物,在静态空的气气氛,以8mW差示扫描量热(DSC)量程,以10℃/min的升温速率,在25-400℃的温度范围下,根据实验所得到的特征和图谱峰进行比较。结果同产地的两种丹参原药材粉末、水提物和醇提物差示扫描量热( DSC)图谱峰形基本一致,仅放热峰温略有不同。结论实验表明差示扫描量热( DSC)法具有试量微样化、不用溶剂、曲线易于解析、快速简便等优点,可作为不同产地丹参及其提取物的鉴别方法之一。

Abstract

Objective Two kinds of Salvia Miltiorrhizae from different sources by differential scanning calorimetry ( DSC) analysis identification,identification in-clude:raw material powder,water extract and alcohol extract.Methods The alpha-A l2O3 as comparative reference substance in the atmosphere,static empty,with a 8 mW differential scanning calorimetry(DSC)range,with 10℃/min heating rate,in the temperature range of 25-400℃,according to the comparison of the characteristics and the spectrum peak.Results Different origin of two kinds of Salvia miltiorrhiza powder ,water and ethanol extracts of differential scanning calorimetry ( DSC) spectrum peak is basically the same,only the exothermic peak temperature slightly different.Conclusion experiments show that the differential scanning calorimetry(DSC)method has a small amount of test sample,no solvent,curve is easy to resolve,quick,can be used as one of the method to identify and extract of Radix Salviae Miltiorrhizae from different habitats.

关键词

差示扫描热/图谱峰/丹参

Key words

Differential scanning calorimetry/Atlas peak/Danshen

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出版年

2014
中国保健营养(上旬刊)
全国卫生产业企业管理协会

中国保健营养(上旬刊)

ISSN:1004-7484
参考文献量5
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