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哈密瓜农药残留检测及风险评估

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为明确哈密瓜样品中的农药残留现状并评估其慢性膳食摄入风险,本研究采用QuEChERS样品前处理方法,结合超高效液相色谱-串联质谱(UPLC-MS/MS)、气相色谱串联质谱(GC-MS/MS),对哈密瓜样品中可能存在的156种农药含量进行测定,并采用慢性膳食摄入风险评估模型进行慢性膳食摄入风险评估.结果表明,哈密瓜样品的农残阳性检出率为81.8%,共检出22种农药.其中,腐霉利和多菌灵的检出率较高,分别为68.2%和45.5%.4~6岁儿童、孕妇及一般人群食用哈密瓜摄入农药的膳食风险均远低于100%.综上,哈密瓜中普遍存在农药残留,但残留水平不高,膳食摄入风险均在可接受范围内,正常食用不会对人体健康造成危害,从而为哈密瓜的质量安全监管提供科学依据,也可为消费者提供参考.
Pesticide Residues Detection and Risk Assessment in Hami cantaloupe
To clarify the current status of pesticide residues in Hami cantaloupe,this study used QuEChERS sample pretreatment method,combined with ultra-high performance liquid chromatography-tandem mass spectrometry(UPLC-MS/MS)and gas chromatography-tandem mass spectrometry(GC-MS/MS),to determined 156 pesticide residues in H.cantaloupe,and conducted a chronic dietary intake risk assessment.The results showed that the detection rate of H.cantaloupe samples was 81.8%,with a total of 22 pesticides detected.Among them,the detection rates of Pythiram and Carbendazim were relatively high,at 68.2%and 45.5%,respectively.The dietary intake risk of residual pesticides for 4-6 children,pregnant woman and general population was all lower than 100%.The results indicated that there were pesticide residues in H.cantaloupe,but the residual level was not high,and the dietary intake risk was within an acceptable range.This study could provide scientific basis for the quality and safety supervision of cantaloupe,and also provided reference data for consumers.

Hami cantaloupeQuEChERSUPLC-MS/MSGC-MS/MSpesticide residue

闫新焕、许敏、刘雪梅、杜文瑜、范艺璇、黄勇平

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中华全国供销合作总社济南果品研究所,山东济南 250220

海南省食品检验检测中心,海南海口 570314

哈密瓜 QuEChERS 超高效液相色谱-串联质谱 气相色谱串联质谱 农药残留

2024

中国果菜
中华全国供销合作总社济南果品研究院 山东省供销合作社联合社 中国果蔬贮藏加工技术研究中心

中国果菜

影响因子:0.204
ISSN:1008-1038
年,卷(期):2024.44(10)