Synthesis of MnV2O6 nanoflakes via simple hydrothermal process

Yi LIU ¹Yitai QIAN²

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作者信息

1. Department of Chemistry,Zaozhuang University,Zaozhuang 277160,China;Department of Chemistry,University of Science and Technology of China,Hefei 230026,China.
2. Department of Chemistry,University of Science and Technology of China,Hefei 230026,China
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Abstract

A single phase of monoclinic MnV2O6 nanoflakes was prepared by a hydrothermal process at 180℃ starting materials and using acetic acid to adjust the pH value of the reaction solution. The as,prepared samples were characterized by field emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM). X,ray photoelectron spectrum (XPS) measurements further confirm the component of MnV2O6.Results indicated that the products consisted of a large quantity of compact accumulated nanoflakes,with average width of 0.85 μtm,thickness of 100 nm and lengths up to 1.7μm.

Key words

MnV2O6/hydrothermal synthesis/nanoflakes

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基金项目

国家高技术研究发展计划(863计划)()

国家重点基础研究发展计划(973计划)(2005CB623601)

出版年

2008

中国化学前沿

高等教育出版社

中国化学前沿

ISSN：1673-3495

参考文献量17

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