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水泥原材料中总铬检测标准方法验证

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为了有效控制水泥中重金属铬,构筑健康的人居环境,准确地检测限制水泥原材料中总铬是非常必要的.对标准方法《水泥原材料中总铬的测定方法》,采用分光光度法测定水泥原材料中总铬含量方法进行了验证.通过分析与研究所测得的线性关系、检出限、精密度,并且计算得出该方法检出限为0.008 9mg/L,相对误差均能满足要求,表明该方法适用于现有水泥生产过程中原材料的检测,在实验室内准确可行.同时对检测实验过程中出现的细节问题提出了操作建议,有助于检测过程细节的规范、完整、准确.
In order to further control the heavy metal chromium in cement and reduce harm to human health,it is necessary to control the total chromium in various raw materials of cement within a limited range.This article validates the spectrophotometric method for determining the total chromium content in cement raw materials,which is studied in the standard method"Determination of Total Chromium in Cement Raw Materials".The linear relationship,detection limit,and precision obtained through analysis and research indicate that this method is suitable for the detection of raw materials in existing cement production processes and is accurate and feasible in the laboratory.And the detection limit of the method is calculated to be 0.0089 mg/L,and the relative error can meet the requirements.This proves that the detection method can be used to detect the total chromium element in cement raw materials and control the chromium content in cement.Improvement suggestions were proposed for the detailed issues that occurred during the testing experiment,making the testing process more standardized,complete,and accurate.

Cement raw materialsSpectrophotometryMethod validation

冯浩、秦洁、和立新、郭强、王路

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冀东水泥铜川有限公司,陕西铜川 727100

水泥原材料 分光光度法 方法验证

2024

中国水泥
中国水泥协会 中国建材技术装备总公司

中国水泥

影响因子:0.153
ISSN:1671-8321
年,卷(期):2024.(1)
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