首页|基于SBSE-GC/MS的荔枝白兰地香气成分分析

基于SBSE-GC/MS的荔枝白兰地香气成分分析

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应用搅拌棒萃取法提取荔枝白兰地中的的香气物质,用峰面积归一法进行定量分析,结合气相色谱-质谱技术及计算机检索技术对分离化合物进行鉴定.荔枝白兰地中香气物质经气相色谱分离共得到65个峰,鉴定出61种物质,占总峰面积的95.81%,对荔枝白兰地香气贡献较大的是酯类60.77%、酸类12.23%、醇类7.62%、苯环衍生物6.13%、酮类化合物4.90%和萜烯类化合物4.53%,香气成分含量较高的前十种物质依次是乙酸乙酯19.02%、2,4-己二烯酸乙酯16.53%、山梨酸10.73%、琥珀酸二乙酯7.70%、辛酸乙酯4.73%、正戊醇4.60%、2,6-二叔丁基对苯甲酚2.25%、苯乙醇2.16%、玫瑰醚2.06%、己酸乙酯1.96%.构成荔枝白兰地香气特征的物质主要是酯类、醇类、酸类、少量的酚类及萜烯类化合物.
Aromatic components analysis in litchi brandy by GS-MS with stir bar sportive extraction
The aroma components of litchi brandy were analyzed by GC-MS with stir bar sportive extraction,and the relative contents were determined by peak normalization method.65 compounds were separated and 61 of them were identified and determined,accounting to 95.81% of the total area of the peaks.Esters compounds contributed most to litchi brandy with the amount of 60.77%,organic acids compounds 12.23%,alcohols compounds 7.62%,benzene derivatives 6.13%,ketone compounds 4.90% and terpene compounds 4.53%.The top ten aroma composition in order was ethyl acetate 19.02%,2,4-hexadienoic acid ethyl ester 16.53%,sorbic acid 10.73%,diethyl butanedioate 7.70%,ethylcaprylate 4.73%,n-amyl alcohol 4.60%,2,6-Di-tert-butyl-4-methylphenol 2.25%,phenethyl alcohol 2.16%,rose oxide 2.06%,ethyl capmate 1.96%.It was found that esters compounds,organic acids compounds,alcohols compounds,terpene compounds and a few phenolic compounds constituted main aroma substance.

litchi brandyaroma componentstir bar sportive extractionGC-MS

卢柯、乔慧、薛楚然、刘树文、徐向文

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西北农林科技大学葡萄酒学院,陕西杨凌712100

广东为多生物科技有限公司,广东茂名525000

荔枝白兰地 香气成分 搅拌棒萃取 气相色谱-质谱法

广东省教育部产学研结合项目资助资金茂名市重大科技专项资助资金

2011A010032009B090300133

2014

中国酿造
中国调味品协会 北京食品科学研究院

中国酿造

CSTPCD北大核心
影响因子:0.759
ISSN:0254-5071
年,卷(期):2014.33(3)
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