首页|基于GC-IMS对不同品种咖啡豆挥发性有机物指纹图谱分析

基于GC-IMS对不同品种咖啡豆挥发性有机物指纹图谱分析

扫码查看
该研究利用顶空气相色谱(HS-GC)-离子迁移谱(IMS)技术对4个不同品种咖啡生豆样品(A1、B1、C1、D1)及其经烘焙后熟豆样品(A2、B2、C2、D2)挥发性风味物质进行检测和分析,并对其进行主成分分析(PCA)。通过构建咖啡GC-IMS风味指纹图谱,比较不同品种咖啡豆挥发性风味物质之间的差异。结果表明,GC-IMS检出104种挥发性风味物质,其中81种风味物质可定性检出。GC-IMS指纹图谱表明,样品D1特征风味物质为丁酸甲酯、乙酸甲酯;样品A2、C2特征风味物质为当归内酯、丁酸乙酯、3-甲基丁醛;样品B2特征风味物质为2-甲基丙烯醛、3-甲基-2-丁烯醛;样品D2特征风味物质为2-呋喃甲硫醇、2,6-二甲基吡啶。PCA结果表明,样品B2、D2及A2、C2距离接近,样品A1、D2距离较远。表明该技术可用于咖啡豆的品种识别、产地追溯和品质控制等方面。
Fingerprint analysis of volatile organic compounds in different varieties ofcoffee beans by gas chromatography-ion mobility spectrometry
In this study,the volatile flavor substances of 4 different varieties of raw coffee beans(A1,B1,C1,D1)and the 4 roasted coffee beans(A2,B2,C2,D2)were tested and analyzed by headspace gas chromatography(HS-GC)-ion migration spectrometry(IMS),and the principal component analysis(PCA)was performed.By constructing GC-IMS flavor fingerprint of coffees,the differences in volatile flavor substances among different va-rieties of coffees were compared.The results showed that 104 volatile flavor substances were detected by GC-IMS,among of which 81 compounds could be qualitatively detected.The GC-IMS fingerprint showed that the characteristic flavor substances of sample D1 were methyl butyrate and methyl acetate,the characteristic flavor substances of samples A2 and C2 were angelica lactone,ethyl butyrate and 3-methylbutyral,the characteristic flavor substances of sample B2 were 2-methylacrolein and 3-methyl-2-butenal,and the characteristic flavor substances of sample D2 were 2-furan-methanethioland 2,6-dimethyl pyridine.PCA results showed that sample B2 was similar to samples D2,A2 and C2,while samples Al and D2 were different,indicating that the technology could be used for variety identification,origin tracing and quality control of coffee beans.

coffee beangas chromatography-ion migration spectrometryvolatile organic compoundfingerprint

杨莉、杨卫星、李茜、樊竹青、李华健、李学玲

展开 >

普洱学院生物与化学学院,云南普洱 665000

云南农业大学食品科学技术学院,云南 昆明 650100

文山州农业科学院,云南文山 663000

咖啡豆 气相色谱-离子迁移谱 挥发性有机物 指纹图谱

云南省教育厅科研项目(2023)普洱学院咖啡研究专项推荐项目(2022)普洱学院青年学术与技术带头人后备人才培养项目

2023J12432022KFZX08QNRC21-04

2024

中国酿造
中国调味品协会 北京食品科学研究院

中国酿造

CSTPCD北大核心
影响因子:0.759
ISSN:0254-5071
年,卷(期):2024.43(1)
  • 27