首页|威士忌制备过程中理化指标及挥发性风味物质动态变化规律研究

威士忌制备过程中理化指标及挥发性风味物质动态变化规律研究

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威士忌是麦芽经糖化、发酵、蒸馏、桶陈等工序制成的蒸馏酒。为明确麦汁发酵及蒸馏过程中理化指标及挥发性风味物质的变化规律,该研究以蒸馏麦芽为原料、以威士忌专用商业酵母为发酵剂制备威士忌。采用高效液相色谱(HPLC)、气相色谱-质谱联用(GC-MS)等技术检测原酒浆发酵及蒸馏过程中理化指标和挥发性风味物质,并基于馏分关键风味物质(气味活度值(OAV)>1)进行主成分分析(PCA)和层次聚类分析(HCA)。结果表明,原酒浆中糖分、酒精度和主要酯类物质在第2天出现拐点;乙酸、丙酸和乳酸含量随着发酵时间增加,在第3天分别达到0。03 g/L、0。13g/L和0。49g/L。通过主成分分析(PCA)和层次聚类分析(HCA)可明显区分馏分。该研究结果可为威士忌发酵工艺优化及酒心摘取提供数据支撑。
Dynamic changes rules of physicochemical indexes and volatile flavor compounds during whisky preparation process
Whiskey is a distilled spirit made from malt by saccharification,fermentation,distillation,barrel aging and other processes.In order to de-termine the changes rules of physicochemical indexes and volatile flavor substances in the process of wort fermentation and distillation,whisky was prepared from malt and commercial yeast.The physicochemical parameters and volatile flavor substances of original liquor pulp during fermentation and distillation process were detected by HPLC and GC-MS,and principal component analysis(PCA)and hierarchical cluster analysis(HCA)were performed based on the key flavor substances of in distillates(odor activity value(OAV)>1).The results showed that sugar,alcohol content and main esters in the original liquor pulp appeared turning points on the 2nd day.The contents of acetic acid,propionic acid and lactic acid increased with the fermentation time,and reached 0.03 g/L,0.13 g/L and 0.49 g/L,respectively,on the 3rd day.PCA and HCA could clearly distinguish distillates.The results could provide data support for whiskey fermentation process optimization and liquor core extraction.

whiskyoriginal liquor pulpphysicochemical indexesdistillatesvolatile flavor compoundsprincipal component analysishierarchical cluster analysis

陈文波、张一、李小燕、杨海莺、牛丽敏、赵凯、李慧

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中粮营养健康研究院有限公司老年营养食品研究北京市工程实验室营养健康与食品安全北京市重点实验室,北京 102209

南京财经大学食品科学与工程学院/江苏省现代粮食流通与安全协同创新中心,江苏南京 210023

河北科技大学 食品与生物学院,河北石家庄 050018

中粮粮谷控股有限公司,北京 100020

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威士忌 原酒浆 理化指标 馏分 挥发性风味物质 主成分分析 层次聚类分析

国家重点研发计划

2021YFD2100904

2024

中国酿造
中国调味品协会 北京食品科学研究院

中国酿造

CSTPCD北大核心
影响因子:0.759
ISSN:0254-5071
年,卷(期):2024.43(2)
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