首页|不同前处理工艺红桔果汁与红桔果酒挥发性风味物质分析

不同前处理工艺红桔果汁与红桔果酒挥发性风味物质分析

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以万州红桔为研究对象,采用带皮和去皮方式榨汁,对浊汁进行酶解澄清处理,分别利用带皮浊汁、带皮清汁、去皮浊汁及去皮清汁酿造红桔果酒。对果酒进行感官评价,同时利用液相色相仪与顶空固相微萃取(HS-SPME)-气相色谱质谱(GC-MS)联用技术测定果酒和果汁样品中有机酸及挥发性风味物质,并基于挥发性风味物质进行主成分分析(PCA)和聚类分析(CA)。结果表明,红桔果汁主要有机酸为苹果酸和柠檬酸,红桔果酒增加了乳酸和乙酸;红桔果汁和红桔果酒中共检测出100种挥发性风味物质,主要化合物包括酯类28种、醇类19种、酚类3种、醚类2种、醛类8种、酮类10种、酸类4种、烷烃类3种及烯烃类23种;总体上,清汁发酵红桔果酒的挥发性风味物质种类较浊汁发酵多,带皮发酵果酒中的醇类和烯烃种类较去皮发酵多。PCA结果表明,不同红桔果汁和红桔果酒样品中主要挥发性风味物质为辛酸乙酯、癸酸乙酯、正己酸乙酯、月桂酸乙酯、棕榈酸乙酯、α-松油醇、苯乙醇、辛醇、香叶醇、麝香草酚、L-紫苏醛、癸醛等;聚类分析结果表明,可将样品聚集为三大类,与PCA分类结果一致。
Analysis of volatile flavor components of red tangerine juice and wine with different pretreatment processes
Taking red tangerinet of Wanzhou as the research object,the juice was extracted by unpeeling and peeling,respectively,and the turbid juice was clarified by enzymatic hydrolysis,the red tangerine wine was brewed with unpeeled turbid juice,unpeeled clear juice,peeled turbid juice and peeled clear juice respectively,and the sensory quality was evaluated.The organic acids and volatile flavor compounds in juice and wine were deter-mined by liquid phase chromatography and headspace solid-phase microextraction(HS-SPME)combined with GC-MS,and principal component anal-ysis(PCA)and cluster analysis(CA)were performed based on volatile flavor components.Results showed that the main organic acids in the juice were malic acid and citric acid,in addition,there were lactic acid and acetic acid in tangerine fruit.A total of 100 volatile flavor components were de-tected in red tangerinet juice and wine,including 28 esters,19 alcohols,3 phenols,2 ethers,8 aldehydes,10 ketones,4 acids,3 alkanes and 23 olefins.In general,there were more types of flavor substances in tangerine wine fermented with clear juice than turbid juice,and there were more types of alco-hols and olefins in fermented wine with unpeeled fermentation than with peeled fermentation.The results of PCA showed that the main volatile flavor substances in different red tangerine juice and wine were ethyl caprylate,ethyl decanoate,ethyl n-caproate,ethyl laurate,ethyl palmitate,α-terpinol,phenyl ethanol,octanol,geraniol,thymol,L-perillaldehyde,capric aldehyde,etc.The results of CA showed that the samples could be clustered into three categories,which were consistent with PCA results.

red tangerine winevolatile flavor componentprincipal component analysiscluster analysis

付勋、聂青玉、张文玲、张艳、李翔、冯婷婷

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重庆三峡职业学院 农林科技学院,重庆 404155

红桔果酒 挥发性风味成分 主成分分析 聚类分析

&&重庆市高等学校创新研究群体项目

CSTB2022TIAD-ZXX0043CXQTP19037

2024

中国酿造
中国调味品协会 北京食品科学研究院

中国酿造

CSTPCD北大核心
影响因子:0.759
ISSN:0254-5071
年,卷(期):2024.43(5)
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