首页|液液萃取结合气质联用技术分析酿酒高粱中的香气成分

液液萃取结合气质联用技术分析酿酒高粱中的香气成分

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该研究通过比较液液萃取、顶空固相微萃取和固相萃取3种前处理方法对酿酒高粱中香气成分的提取效果,建立了基于液液萃取结合气相色谱-质谱(GC-MS)联用分析酿酒高粱中香气成分的方法。结果表明,采用液液萃取结合GC-MS检出酿酒高粱挥发性风味物质最多,为37种,其中,醛类15种、酮类4种、醇类8种、酯类6种、环类化合物3种,酸类1种。其中相对含量较高的化合物有2-庚烯醛(19。71%)、己醛(16。08%)、(Z)-2-癸烯醛(8。57%)和2-戊基呋喃(6。04%),同时还检出壬醛、1-辛烯-3-醇、γ-壬内酯等香气阈值较低的化合物。
Analysis of aroma components in brewing sorghum by liquid-liquid extraction combined with GC-MS
By comparing the extraction effects of 3 pretreatment methods,namely liquid-liquid extraction,headspace solid-phase microextraction and solid-phase extraction on aroma components in brewing sorghum,a method based on liquid-liquid extraction combined with gas chromatography-mass spectrometry(GC-MS)was established for the analysis of aroma components in brewing sorghum.The results showed that a total of 37 volatile flavor compounds were detected by liquid-liquid extraction combined with GC-MS,including 15 aldehydes,4 ketones,8 alcohols,6 esters,3 cyclic compounds and 1 acid compound.The compounds with high relative content were 2-heptenal(19.71%),hexal(16.08%),(Z)-2-decenoal(8.57%)and 2-amylfuran(6.04%).Meanwhile,some compounds with low aroma threshold were also detected,such as nonanal,l-octene-3-ol,γ-nonolactone,etc.

brewing sorghumvolatile flavor compoundsliquid-liquid extractionGC-MS

胡娇、李松柏、宋廷富、罗珠、李杨华、郑佳

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宜宾五粮液股份有限公司,四川宜宾 644000

固态发酵资源利用四川省重点实验室,四川 宜宾 644000

中国轻工业浓香型白酒固态发酵重点实验室,四川 宜宾 644000

酿酒高粱 挥发性风味物质 液液萃取 气相色谱-质谱法

四川省科技计划项目

2019ZYZF0092

2024

中国酿造
中国调味品协会 北京食品科学研究院

中国酿造

CSTPCD北大核心
影响因子:0.759
ISSN:0254-5071
年,卷(期):2024.43(7)
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