首页|甘谷伏椒挥发油成分及抗氧化活性研究

甘谷伏椒挥发油成分及抗氧化活性研究

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甘谷伏椒是重要的调味品之一.文章采用水蒸气蒸馏法,利用正交试验设计,详细考察了甘谷伏椒挥发油的提取工艺条件.同时,采用气相色谱-质谱联用技术对所提取的挥发油的化学成分进行了鉴定和分析,并重点研究了挥发油对羟基自由基和DPPH自由基的清除能力.结果表明,水蒸气蒸馏法提取甘谷伏椒挥发油的最佳提取条件为料液比1∶10、浸泡时间4 h、蒸馏时间5 h.从挥发油中分析鉴定出41种化学成分,主要为γ-松油烯、E,E-金合欢醇乙酸酯、异松油烯、顺式-香叶醇等,其中不饱和烃类物质占挥发油成分的94.01%.抗氧化试验表明,挥发油具有较好的抗氧化能力,对羟基自由基和DPPH自由基均有较好的清除效果,最高清除率分别达到73.2%和93.9%.因此,甘谷伏椒挥发油具有较强的抗氧化功效,在调味品领域具有重要的应用价值.
Study on Components and Antioxidant Activity of Volatile Oil from Gangu Fujiao
:Gangu Fujiao is one of the important condiments.In this paper,the extraction process conditions of volatile oil from Gangu Fujiao are investigated in detail using steam distillation method and orthogonal test design.At the same time,the chemical components of the extracted volatile oil are determined and analyzed by GC-MS,and the scavenging capacity of the volatile oil on hydroxyl radicals and DPPH radicals is studied.The results show that the optimal conditions for the extraction of volatile oil from Gangu Fujiao by steam distillation method are as follows:solid-liquid ratio is 1∶10,soaking time is 4 h and distillation time is 5 h.There are 41 kinds of chemical components identified in the volatile oil and the main components are γ-terpinene,E,E-acacia alcohol acetate,terpinolene,cis-geraniol and so on.Among them,unsaturated hydrocarbons account for 94.01%of volatile oil components.The antioxidant test indicates that the volatile oil has good antioxidant capacity and good scavenging effects on hydroxyl radicals and DPPH radicals,with the highest scavenging rates of 73.2%and 93.9%respectively.Therefore,volatile oil from Gangu Fujiao has strong antioxidant function and important application value in the field of condiments.

Gangu Fujiaovolatile oilsteam distillation methodchemical componentsantioxidant activity

陶静、翁霞、王喜珠

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鞍山师范学院化学与生命科学学院,辽宁鞍山 114007

辽宁省天然产物活性分子开发及利用重点实验室,辽宁鞍山 114007

甘谷伏椒 挥发油 水蒸气蒸馏法 化学成分 抗氧化活性

辽宁省百千万人才工程项目辽宁省自然科学基金面上项目鞍山师范学院校企合作项目

2019921009201602001PAN2018011

2024

中国调味品
全国调味品科技情报中心站

中国调味品

CSTPCD北大核心
影响因子:0.541
ISSN:1000-9973
年,卷(期):2024.49(4)
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