中国调味品2024,Vol.49Issue(4) :109-115.DOI:10.3969/j.issn.1000-9973.2024.04.018

双斑东方鲀鱼头美拉德反应工艺优化及挥发性风味物质分析

Optimization of Maillard Reaction Process of Takifugu bimaculatus Head and Analysis of Volatile Flavor Substances

刘瑞 刘智禹 陈贝 方旭波 张瑞娟 陈小娥
中国调味品2024,Vol.49Issue(4) :109-115.DOI:10.3969/j.issn.1000-9973.2024.04.018

双斑东方鲀鱼头美拉德反应工艺优化及挥发性风味物质分析

Optimization of Maillard Reaction Process of Takifugu bimaculatus Head and Analysis of Volatile Flavor Substances

刘瑞 1刘智禹 2陈贝 2方旭波 3张瑞娟 3陈小娥4
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作者信息

  • 1. 浙江海洋大学食品与药学学院,浙江舟山 316022;福建省海洋生物增养殖与高值化利用重点实验室,福建厦门 361013
  • 2. 福建省海洋生物增养殖与高值化利用重点实验室,福建厦门 361013
  • 3. 浙江国际海运职业技术学院,浙江舟山 316024
  • 4. 浙江海洋大学食品与药学学院,浙江舟山 316022
  • 折叠

摘要

为了提高双斑东方鲀鱼头的附加值,制备了河鲀鱼风味基料.以鱼头为原料,酶解后利用美拉德反应对其进行增香、呈色,采用正交试验优化工艺条件,并利用气相色谱-质谱(gas chromatography-mass spectrometry,GC-MS)联用技术和电子鼻分析美拉德反应前、后挥发性物质的变化.结果表明,双斑东方鲀鱼头酶解液美拉德反应的最适条件为木糖-氨基葡萄糖配比1∶2、还原糖添加量3.5%、反应时间65 min、反应温度115 ℃.GC-MS结果显示,美拉德反应改善了酶解液的整体风味,醛类是美拉德反应产物中最主要的挥发性物质,其他化合物则使其风味更加丰富.电子鼻雷达图分析结果与GC-MS数据结果基本保持一致.该研究结果为以双斑东方鲀鱼头为原料开发海鲜风味基料提供了理论基础.

Abstract

In order to improve the added value of Takifugu bimaculatus head,the pufferfish flavor basic material is prepared.With fish head as the raw material,after enzymatic hydrolysis,Maillard reaction is used to enhance its aroma and color.The process conditions are optimized by orthogonal test.The changes of volatile substances before and after Maillard reaction are analyzed by gas chromatography-mass spectrometry(GC-MS)and electronic nose.The results show that the optimum conditions for Maillard reaction of Takifugu bimaculatus head enzymatic hydrolysate are as follows:xylose-glucosamine ratio is 1∶2,the addition amount of reducing sugar is 3.5%,reaction time is 65 min and reaction temperature is 115 ℃.The results of GC-MS show that Maillard reaction improves the overall flavor of enzymatic hydrolysate.Aldehydes are the main volatile substances in Maillard reaction products,and other compounds make the flavor richer.The analysis results of electronic nose radar diagram are basically consistent with the results of GC-MS data.The results of this study have provided a theoretical basis for the development of seafood flavor basic material with Takifugu bimaculatus head as the raw material.

关键词

双斑东方鲀鱼头/美拉德反应/正交试验/风味/GC-MS/电子鼻

Key words

Takifugu bimaculatus head/Maillard reaction/orthogonal test/flavor/GC-MS/electronic nose

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基金项目

福建省海洋生物增养殖与高值化利用重点实验室开放基金(2020fjscq02)

出版年

2024
中国调味品
全国调味品科技情报中心站

中国调味品

CSTPCD北大核心
影响因子:0.541
ISSN:1000-9973
参考文献量26
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