首页|基于电子舌、GC-IMS和GC-MS分析桂林米粉卤水的风味特征

基于电子舌、GC-IMS和GC-MS分析桂林米粉卤水的风味特征

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该研究采用电子舌分析技术结合气相色谱-离子迁移谱联用技术(gas chromatography-ion mobility spectrometry,GC-IMS)对南宁和桂林两市18个桂林米粉餐饮店的卤水及两款产业化卤水进行检测,经滋味轮廓、指纹图谱、挥发性物质相似度分析,选择5个典型样品,通过顶空固相微萃取-气相色谱-质谱联 用技术(headspace solid-phase microextraction-gas chromatography-mass spectrometry,HS-SPME-GC-MS)结合气味活性值(odor activity value,OAV)确定关键风味物质.电子舌结果显示:桂林米粉卤水的滋味特征为咸味、鲜味明显,鲜味回味突出,有轻微苦涩味,并伴有一定苦味回味;GC-IMS结果显示:18家桂林米粉餐饮店的卤水中共有挥发性物质60种(定性出37种),且具有一定相似性,但与两款产业化卤水的挥发性成分有明显差异;GC-MS共鉴定出84种挥发性物质,其中烯烃类、醇类、醛类、酯类、醚类和杂环类化合物为桂林米粉卤水主要的挥发性成分;丁香酚、对烯丙基苯甲醚、茴香醚为5个桂林米粉卤水样品共有的关键风味物质.
Analysis of Flavor Characteristics of Brine of Guilin Rice Noodles Based on Electronic Tongue,GC-IMS and GC-MS
In this study,electronic tongue analysis technology combined with gas chromatography-ion migration spectrometry(GC-IMS)is used to detect the brine of 18 Guilin rice noodles restaurants in Nanning and Guilin,as well as two types of industrial brine.After taste profile,fingerprint and similarity analysis of volatile substances,five typical samples are selected,and headspace solid-phase microextraction-gas chromatography-mass spectrometry(HS-SPME-GC-MS)combined with odor activity value(OAV)is used to determine the key flavor substances.Electronic tongue results show that the taste characteristics of brine of Guilin rice noodles are significant saltiness and umami,with prominent umami aftertaste,slight bitterness and astringency and a certain bitterness aftertaste.GC-IMS results show that there are a total of 60 volatile substances in the brine from 18 Guilin rice noodles restaurants(37 substances are identified by qualitative analysis),and they have some similarities,but they are significantly different from the volatile components of two types of industrialized brine.By using GC-MS,a total of 84 volatile substances are identified,among which,alkenes,alcohols,aldehydes,esters,ethers and heterocyclic compounds are the main volatile components in the brine of Guilin rice noodles.Eugenol,p-allylanisole and anisole are the key flavor substances shared by five Guilin rice noodle brine samples.

brine of Guilin rice noodlesvolatile componentselectronic tonguegas chromatography-ion migration spectrometryheadspace solid-phase microextraction-gas chromatography-mass spectrometry

周杰、姜洁群、马瑞东、覃静凯、陈梅、覃忠意、刘小玲

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广西大学轻工与食品工程学院,南宁 530004

广西高校特色农产品精深加工与安全控制重点实验室,南宁 530004

桂林米粉卤水 挥发性成分 电子舌 气相色谱-离子迁移谱 顶空固相微萃取-气相色谱-质谱联用

2024

中国调味品
全国调味品科技情报中心站

中国调味品

CSTPCD北大核心
影响因子:0.541
ISSN:1000-9973
年,卷(期):2024.49(7)
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