中国有色金属学报(英文版)2024,Vol.34Issue(10) :3208-3220.DOI:10.1016/S1003-6326(24)66603-3

增材制造异构组织TiAl合金热压缩过程中的显微组织演变及动态再结晶机制

Microstructural evolution and dynamic recrystallization mechanisms of additively manufactured TiAl alloy with heterogeneous micro structure during hot compression

陶慧 李慧中 李佳慧 王丽 贺卫卫 谭孝芬 周睿 梁霄鹏
中国有色金属学报(英文版)2024,Vol.34Issue(10) :3208-3220.DOI:10.1016/S1003-6326(24)66603-3

增材制造异构组织TiAl合金热压缩过程中的显微组织演变及动态再结晶机制

Microstructural evolution and dynamic recrystallization mechanisms of additively manufactured TiAl alloy with heterogeneous micro structure during hot compression

陶慧 1李慧中 2李佳慧 1王丽 3贺卫卫 4谭孝芬 1周睿 5梁霄鹏2
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作者信息

  • 1. 中南大学材料科学与工程学院,长沙 410083
  • 2. 中南大学材料科学与工程学院,长沙 410083;中南大学粉末冶金国家重点实验室,长沙 410083;中南大学有色金属材料科学与工程教育部重点实验室,长沙 410083
  • 3. 中南大学粉末冶金国家重点实验室,长沙 410083
  • 4. 西安赛隆增材技术股份有限公司,西安 710016
  • 5. 香港城市大学材料科学与工程系,香港高等研究院,香港九龙 999077
  • 折叠

摘要

采用热压缩实验、光学显微镜(OM)、扫描电镜(SEM)、电子背散射衍射(EBSD)和透射电镜(TEM)研究了电子束选区熔化(SEBM)制备的Ti-48Al-2Cr-2Nb合金(摩尔分数,%)在1150 ℃和0.1 s-1条件下热变形过程中的显微组织演变和动态再结晶(DRX)机制.结果表明:合金的初始显微组织为沿打印方向交替分布的γ粗晶层和γ+α2+(α2/γ)细晶层.热变形初期,粗晶中形成有利于后续变形的变形孪晶,细晶区域发生少量动态再结晶(DRX).随着应变的增加,粗晶区和细晶区通过不同的再结晶机制形成大量的DRX晶粒.其中,细晶区的DRX机制为不连续动态再结晶(DDRX),粗晶区的DRX机制包括DDRX和连续动态再结晶(CDRX).

Abstract

Microstructural evolution and dynamic recrystallization(DRX)mechanisms of a Ti-48Al-2Cr-2Nb(at.%)alloy prepared by selective electron beam melting(SEBM)during hot deformation at 1150 ℃ and 0.1 s-1 were investigated by hot compression tests,optical microscope(OM),scanning electron microscope(SEM),electron back-scattered diffraction(EBSD)and transmission electron microscope(TEM).The results show that the initial microstructure of the as-SEBMed alloy exhibits layers of coarse y grains and fine γ+α2+(α2/γ)lamellar mixture grains alternately along the building direction.During the early stage of hot deformation,deformation twins tend to form within the coarse grains,facilitating subsequent deformation,and a small number of DRX grains appear in the fine-grained regions.With the increase of strain,extensive DRX grains are formed through different DRX mechanisms in both coarse and fine-grained regions,involving discontinuous dynamic recrystallization mechanism(DDRX)in the fine-grained regions and a coexistence of DDRX and continuous dynamic recrystallization(CDRX)in the coarse-grained regions.

关键词

TiAl合金/电子束选区熔化/异构组织/不连续动态再结晶/连续动态再结晶

Key words

TiAl alloy/selective electron beam melting/heterogeneous microstructure/discontinuous dynamic recrystallization(DDRX)/continuous dynamic recrystallization(CDRX)

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基金项目

Shaanxi Province Key Research and Development Projects,China(2023KXJ-071)

National Natural Science Foundation of China(52274402)

National Natural Science Foundation of China(52174381)

出版年

2024
中国有色金属学报(英文版)
中国有色金属学会

中国有色金属学报(英文版)

CSTPCDCSCD
影响因子:1.183
ISSN:1003-6326
参考文献量44
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