首页|冷却速率对7050铝合金淬火析出行为的影响

冷却速率对7050铝合金淬火析出行为的影响

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基于末端淬火的高通量实验,结合扫描电子显微镜(SEM)、电子背散射衍射(EBSD)、透射电子显微镜(TEM)、高分辨率透射电子显微镜(HRTEM)和扫描透射电子显微镜(STEM)研究了7050铝合金的淬火析出行为.结果表明:随着冷却速率的降低,电导率增加,淬火析出相的种类和形核位置均增加.有利形核析出的位置顺序为大角度晶界、小角度晶界(亚晶界)、再结晶晶内(Al3Zr粒子)、位错和亚晶内(Al3Zr粒子).淬火析出相的析出顺序为η相、S相、T相和Y相.随冷却速率的降低,η相依次在大角度晶界、小角度晶界、再结晶晶内(Al3Zr粒子)和部分亚晶内析出;当冷却速率低于630℃/min时,S相在亚晶(界)析出,T相在再结晶晶内(Al3Zr粒子)和高位错密度的亚晶(界)处析出;当冷却速率低于164℃/min时,Y相在亚晶的位错处析出,η相和T相也在亚晶内析出.
Effect of cooling rate on quenching precipitation behavior of 7050 aluminum alloy
The quenching precipitation behavior of 7050 aluminum alloy was studied by high-throughput experiment based on end-quenching,combined with scanning electron microscopy(SEM),electron backscattering diffraction(EBSD),transmission electron microscopy(TEM),high-resolution transmission electron microscopy(HRTEM)and scanning transmission electron microscopy(STEM).The results show that,with the decrease of cooling rate,the electrical conductivity increases,and the types and nucleation locations of quenching precipitates increase.The position order of favorable nucleation precipitation is high angle grain boundary,low angle grain boundary(subgrain boundary),recrystallization grain(Al3Zr particles),dislocation and subgrain(Al3Zr particles).The precipitation sequence of the quenching precipitated phase is η phase,S phase,T phase and Y phase.With the decrease of cooling rate,η phase precipitates in high angle grain boundaries,low angle grain boundaries,recrystallization(Al3Zr particles)and part of subgrains successively.When the cooling rate rate is lower than 630℃/min,the S phase precipitates in subgrains(boundaries),and the T phase precipitates in recrystallized grains(Al3Zr particles)and subgrains(boundaries)with high dislocation density.When the cooling rate is lower than 164℃/min,Y phase precipitates at the dislocation of subgrains,η phase and T phase also precipitate inside subgrains.

7050 alloyend quenchingmicrostructureheterogeneous precipitation

李承波、赵偲、肖博、朱戴博、张新明

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湘潭大学 机械工程与力学学院,湘潭 411105

中南大学 材料科学与工程学院,长沙 410083

广东兴发铝业有限公司,佛山 5281371

7050铝合金 末端淬火 显微组织 非均匀析出

国家自然科学基金广西壮族自治区科技重大专项广东省重点实验室开放基金

52205421桂科AA23023028XF20230330-XT

2024

中国有色金属学报
中国有色金属学会

中国有色金属学报

CSTPCD北大核心
影响因子:1.108
ISSN:1004-0609
年,卷(期):2024.34(3)
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