首页|C70250铜合金连续挤压-冷轧-时效工艺过程中的显微组织及性能

C70250铜合金连续挤压-冷轧-时效工艺过程中的显微组织及性能

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本文以直径为25 mm的C70250合金杆为原材料,对该合金进行320 mm×14 mm大宽幅U型连续挤压板坯及后续冷轧、时效工艺研究,旨在探索一种高强高导铜合金新型短流程制备技术。首先利用有限元模拟方法对C70250合金连续挤压过程关键场量进行分析,然后进行试验研究。采用光学显微镜(OM)、扫描电子显微镜(SEM)、电子背散射衍射(EBSD)对合金各道次样品进行显微组织分析,利用显微硬度仪、万能试验机和电导率测量仪进行性能测试。结果表明:经过连续挤压后,晶粒发生明显的细化和均匀化,基体中有少量Ni2Si相析出,导电率由37。47%IACS下降到30。27%IACS,硬度由88。0HV提高至108。9HV;板坯在横向上由边部到心部,晶粒尺寸逐渐减小,硬度逐渐增大,沿挤压方向的显微组织及硬度分布均匀,在厚度方向上晶粒尺寸从表面到心部逐渐增大,其硬度心部硬度较低,接近上下表面位置的硬度较高;经过冷轧的带材形成纤维组织并伴随晶粒碎化,经时效处理后,合金带材综合性能得到大幅提升。对U型连续挤压后的板坯进行变形量87。5%冷轧-(450℃,1 h)预时效+变形量66。7%冷轧-(350℃,2 h)时效处理后,得到的合金带材硬度达到233。8 HV,导电率达到47。82%IACS,抗拉强度为688。0 MPa,伸长率为10。2%。
Microstructure and properties of C70250 copper alloy during continuous extrusion-cold rolling-aging process
In this paper,C70250 alloy rod with diameter of 25 mm was used as raw material,and the 320 mm× 14 mm large-width U-shaped continuous extrusion slab and the subsequent cold rolling and aging process of the alloy were studied,aiming to explore a new short-process preparation technology for high-strength and high-conductivity copper alloy. Firstly,the finite element simulation method was used to analyze the key field quantities of C70250 alloy in the continuous extrusion process,and then the experimental study was carried out. The optical microscopy (OM),scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD) were used to analyze the microstructure of the alloy samples,and the performance tests were carried out by the microhardness tester,universal testing machine and conductivity measuring instrument. The results show that the grain is significantly refined and homogenized after continuous extrusion,a small amount of Ni2Si phase is precipitated in the matrix,the conductivity decreases from 37.47%IACS to 30.27%IACS,and the hardness increases from 88.0HV to 108.9 HV. The grain size of the slab gradually decreases from the edge to the core in the transverse direction,the hardness gradually increases,the microstructure and hardness are evenly distributed along the extrusion direction,and the grain size gradually increases from the surface to the core in the thickness direction,and its hardness core is low at the center and high at the position and near the upper and lower surface. The fiber structure of strip after cold-rolled is formed and accompanied by grain fragmentation,and the comprehensive performance of the alloy strip is greatly improved after aging treatment. The alloy strip prepared by the U-shaped continuous extruded slab is treated by cold rolling with deformation 87.5%-(450 ℃,1 h) pre-aging+cold rolling with deformation 66.7%-(350 ℃,2 h) aging,the hardness reaches 233.8HV,the conductivity reaches 47.82%IACS,the tensile strength is 688.0 MPa,and the elongation is 10.2%.

C70250 copper alloycontinuous extrusioncold rollingaging treatmentmicrostructureproperty

梁海成、高博伦、王松伟、邓偲瀛、陈帅峰、刘劲松

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沈阳理工大学材料科学与工程学院,沈阳 110159

中国科学院金属研究所师昌绪先进材料创新中心,沈阳 110016

C70250铜合金 连续挤压 冷轧 时效处理 显微组织 性能

2024

中国有色金属学报
中国有色金属学会

中国有色金属学报

CSTPCD北大核心
影响因子:1.108
ISSN:1004-0609
年,卷(期):2024.34(12)