中国油脂2024,Vol.49Issue(9) :10-15.DOI:10.19902/j.cnki.zgyz.1003-7969.230670

超临界二氧化碳萃取元宝枫籽油工艺优化

Optimization of supercritical carbon dioxide extraction of Acer truncatum seed oil

蒋雨桥 赵仲恺 张文斌
中国油脂2024,Vol.49Issue(9) :10-15.DOI:10.19902/j.cnki.zgyz.1003-7969.230670

超临界二氧化碳萃取元宝枫籽油工艺优化

Optimization of supercritical carbon dioxide extraction of Acer truncatum seed oil

蒋雨桥 1赵仲恺 2张文斌1
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作者信息

  • 1. 江南大学 食品学院,江苏 无锡 214122
  • 2. 新疆大学 生命科学与技术学院,乌鲁木齐 830046
  • 折叠

摘要

为了得到品质优良的元宝枫籽油产品,采用超临界二氧化碳萃取元宝枫籽油,以油脂萃取率为指标,通过单因素试验和响应面试验优化工艺条件,并对所得元宝枫籽油的脂肪酸组成、理化指标、甾醇和生育酚含量进行分析.结果表明:超临界二氧化碳萃取元宝枫籽油的最优工艺条件为原料粒度380~830 μm(20~40 目)、二氧化碳流量28 L/h、萃取温度37℃、萃取压力44 MPa、萃取时间100 min,在该条件下油脂萃取率达(98.7±0.2)%;元宝枫籽油中神经酸含量高达9.34%,总不饱和脂肪酸含量为86.7%,各项理化指标均符合相关标准,总甾醇和总生育酚含量分别为988.1 μg/g和991.4 μg/g,综合品质优于正己烷萃取和低温压榨制取的油脂.综上,超临界二氧化碳萃取元宝枫籽油的萃取率高,产品品质优良,是一种绿色、高效的提油技术.

Abstract

In order to obtain high-quality Acer truncatum seed oil,the supercritical carbon dioxide extraction method was used to extract Acer truncatum seed oil,and the process conditions were optimized through single factor experiment and response surface methodology using the oil extraction rate as an indicator.The fatty acid composition,physicochemical indexes,and contents of sterol and tocopherol of the Acer truncatum seed oil were analyzed.The results showed that the optimal process conditions for supercritical carbon dioxide extraction of Acer truncatum seed oil were particle size 380-830 μm(20-40 meshes),carbon dioxide flow rate 28 L/h,extraction temperature 37℃,extraction pressure 44 MPa,and extraction time100 min.Under these conditions,the oil extraction rate reached(98.7±0.2)%.The nervonic acid content in Acer truncatum seed oil was as high as 9.34%,and the total unsaturated fatty acid content was 86.7%.The physicochemical indexes of Acer truncatum seed oil were in line with the relevant standards,and its total sterol and total tocopherol contents were 988.1 μg/g and 991.4 μg/g,respectively.The comprehensive quality of Acer truncatum seed oil extracted by supercritical carbon dioxide extraction was better than that of the oil extracted by hexane extraction and low-temperature pressing.In summary,the supercritical carbon dioxide extraction method has a high oil extraction rate and excellent product quality,which is a green and efficient oil extraction technology.

关键词

元宝枫籽油/超临界二氧化碳萃取/脂肪酸组成/油脂品质

Key words

Acer truncatum seed oil/supercritical carbon dioxide extraction/fatty acid composition/oil quality

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基金项目

"十四五"国家重点研发计划(2021YFD2100301-04)

新疆维吾尔自治区重大科技专项(2022A02009-4)

出版年

2024
中国油脂
国家粮食储备局西安油脂科学研究设计院

中国油脂

CSTPCD北大核心
影响因子:0.842
ISSN:1003-7969
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