首页|玻纤耐火砖的加压浸出工艺研究

玻纤耐火砖的加压浸出工艺研究

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试验对某玻纤厂产出的废耐火砖进行加压酸浸处理,探索最佳浸出工艺条件。试验结果表明,当耐火砖用量为 100 g,液固比为 5∶1,盐酸用量为 80 mL,硝酸用量为 20 mL,反应温度为 200℃,压强为1。6 MPa,反应时间为 4 h时,铂的浸出率可达 99。05%,铑的浸出率可达 98。21%,渣中铂含量和铑含量分别降低至 0。001 6%、0。000 3%。在最佳浸出工艺条件下,采用低浓度盐酸+硝酸混酸体系,加压浸出可实现铂和铑的高效浸出,具有较好的应用前景。
Research on Pressure Leaching Process of Fiberglass Refractory Bricks
The experiment conducts pressurized acid leaching treatment on waste refractory bricks produced by a fiberglass factory,exploring the optimal leaching process conditions.The experimental results show that when the amount of refractory brick is 100 g,the liquid-solid ratio is 5∶1,the amount of hydrochloric acid is 80 mL,the amount of nitric acid is 20 mL,the reaction temperature is 200℃,the pressure is 1.6 MPa,and the reaction time is 4 h,the leaching rate of platinum can reach 99.05%,and the leaching rate of rhodium can reach 98.21%,and the platinum content and rhodium content in the slag are reduced to 0.001 6%and 0.000 3%,respectively.Under the optimal leaching process conditions,using a low concentration hydrochloric acid+nitric acid mixed acid system,pressure leaching can achieve efficient leaching of platinum and rhodium,which has good application prospects.

fiberglass refractory brickspressure leachingplatinumrhodium

张帆、刘贵清、吴祖璇、张金池、刘昱辰

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江苏北矿金属循环利用科技有限公司,江苏 徐州 221006

玻纤耐火砖 加压浸出

2024

中国资源综合利用
徐州北矿金属循环利用研究所 中国物资再生协会

中国资源综合利用

CHSSCD
影响因子:0.358
ISSN:1008-9500
年,卷(期):2024.42(2)
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