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气相色谱-质谱法测定酒店空气中7种苯系物

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试验运用气相色谱-质谱法测定扩建装修酒店空气中7种苯系物,采用活性炭管采样和二硫化碳解吸,同时对质谱参数和色谱柱进行优化。结果表明,色谱柱能有效分离苯系物中 7 种待测组分,实现各组分峰完全分离。苯系物具有良好线性关系,相关系数R2>0。999,检出限介于 0。60~2。20 μg/L,加标回收率为 93。9%~98。2%,相对标准偏差为 1。8%~4。0%,准确度和精密度良好。苯系物质量控制样品测定表明,该方法符合质控范围。气相色谱-质谱法可用于检测酒店空气中 7 种苯系物,方法准确可靠,灵敏度高。
Determination of 7 Benzene Derivatives in Hotel Air by Gas Chromatography-Mass Spectrometry
The experiment uses gas chromatography-mass spectrometry to determine 7 benzene derivatives in the air of expanded and renovated hotels,and uses activated carbon tubes for sampling and carbon disulfide for desorption,while optimizing mass spectrometry parameters and chromatographic columns.The results indicate that the chromatographic column can effectively separate the 7 components to be tested in benzene derivatives,achieving complete peak separation of each component.Benzene derivatives have a good linear relationship,the correlation coefficient R2 is greater than 0.999,and the detection limit is 0.60~2.20 μg/L,and the recovery rate of spiking is 93.9%~98.2%,and the relative standard deviation is 1.8%~4.0%,indicating good accuracy and precision.The determination of quality control samples for benzene derivatives indicates that this method meets the quality control range.Gas chromatography-mass spectrometry can be used to detect 7 benzene derivatives in hotel air,which is accurate,reliable,and highly sensitive.

gas chromatography-mass spectrometrychromatographic columnbenzene derivativesairhotels

周珊

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宁德市疾病预防控制中心,福建 宁德 352100

气相色谱-质谱法 色谱柱 苯系物 空气 酒店

2024

中国资源综合利用
徐州北矿金属循环利用研究所 中国物资再生协会

中国资源综合利用

CHSSCD
影响因子:0.358
ISSN:1008-9500
年,卷(期):2024.42(2)
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