首页|磁性Fe3O4/莫来石陶粒复合材料制备研究

磁性Fe3O4/莫来石陶粒复合材料制备研究

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煤矸石是煤炭开采和洗选过程排放的固体废弃物,是我国目前年排放量和累计堆存量最大的工业废渣。煤矸石可用于制备重金属吸附材料,实现以废治废。试验将煤矸石在 1 200℃温度下烧结制成陶粒,然后将陶粒在不同浓度的硝酸铁溶液中浸渍,分离陶粒并烘干,用管式炉对其进行氢气还原处理,得到磁性Fe3O4/莫来石陶粒复合材料,研究陶粒复合材料的物相、微观形貌、磁性能及密度。结果表明,陶粒负载物的物相组成为Fe3O4,作为前驱体溶液,硝酸铁溶液浓度越大,陶粒复合材料磁性越强,证实负载工艺可行。
Study on Preparation of Magnetic Fe3O4/Mullite Ceramic Particle Composite Materials
Coal gangue is the solid waste discharged during coal mining and washing processes,and is currently the largest industrial waste residue in China in terms of annual emissions and cumulative storage.Coal gangue can be used to prepare heavy metal adsorption materials,achieving waste treatment by waste.The experiment sinters coal gangue into ceramic particles at a temperature of 1 200℃,then immerses the ceramic particles in different concentrations of iron nitrate solution,separates the ceramic particles and dries them,and uses a tube furnace for hydrogen reduction treatment to obtain magnetic Fe3O4/mullite ceramic particle composite materials,and studies the phase,microstructure,magnetic properties,and density of the ceramic particle composite materials.The results show that the phase composition of the ceramic particle loaded material is Fe3O4,as a precursor solution,the higher the concentration of iron nitrate solution,the stronger the magnetic properties of the ceramic particle composite material,confirming the feasibility of the loading process.

coal gangueceramic composite materialspreparationmagnetismFe3O4mullite

吉国荣、郝惠兰、高云峰、丰铭、朱保顺、田玉明

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山西科技学院材料科学与工程学院,山西 晋城 048011

太原科技大学材料科学与工程学院,太原 030024

煤矸石 陶粒复合材料 制备 磁性 Fe3O4 莫来石

晋城市重点研发项目晋城市重点研发项目山西科技学院校级科研项目山西科技学院科研启动经费项目

2022010220220104XKY0102024011

2024

中国资源综合利用
徐州北矿金属循环利用研究所 中国物资再生协会

中国资源综合利用

CHSSCD
影响因子:0.358
ISSN:1008-9500
年,卷(期):2024.42(7)