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电感耦合等离子体质谱法测定水中13种金属元素

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以电感耦合等离子体质谱仪为分析仪器,建立水中 13 种金属元素的分析方法.试验结果表明:建立的方法各种金属元素校准曲线线性良好,相关系数均大于 0.999;检出限低,为 0.01~0.26 μg/L;相对标准偏差小,均小于 3%;准确度高,加标回收率在 92.3%~105.9%.该方法适合环境水样的日常检测.
Determination of 13 Metal Elements in Water by Inductively Coupled Plasma Mass Spectrometry
An inductively coupled plasma mass spectrometer was used as the analytical instrument to establish the analytical methods for 13 metal elements in water.The results showed that:the calibration curves of the established method were linear with the correlation coefficients greater than 0.999;the detection limits were low,ranging from 0.01~0.26 μg/L;the relative standard deviations were small,all of them were less than 3%;and the accuracy was high,with the recoveries of spiked standards in the range of 92.3%~105.9%.The method is suitable for the routine testing of environmental water samples.

inductively coupled plasma mass spectrometrymetal elementwater

夏海军、凌晨慧、郝露露

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安徽省宣城生态环境监测中心,安徽 宣城 242000

电感耦合等离子体质谱仪 金属元素

2024

中国资源综合利用
徐州北矿金属循环利用研究所 中国物资再生协会

中国资源综合利用

CHSSCD
影响因子:0.358
ISSN:1008-9500
年,卷(期):2024.42(7)