中国资源综合利用2024,Vol.42Issue(7) :48-51.DOI:10.3969/j.issn.1008-9500.2024.07.013

电感耦合等离子体质谱法测定水中13种金属元素

Determination of 13 Metal Elements in Water by Inductively Coupled Plasma Mass Spectrometry

夏海军 凌晨慧 郝露露
中国资源综合利用2024,Vol.42Issue(7) :48-51.DOI:10.3969/j.issn.1008-9500.2024.07.013

电感耦合等离子体质谱法测定水中13种金属元素

Determination of 13 Metal Elements in Water by Inductively Coupled Plasma Mass Spectrometry

夏海军 1凌晨慧 1郝露露1
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作者信息

  • 1. 安徽省宣城生态环境监测中心,安徽 宣城 242000
  • 折叠

摘要

以电感耦合等离子体质谱仪为分析仪器,建立水中 13 种金属元素的分析方法.试验结果表明:建立的方法各种金属元素校准曲线线性良好,相关系数均大于 0.999;检出限低,为 0.01~0.26 μg/L;相对标准偏差小,均小于 3%;准确度高,加标回收率在 92.3%~105.9%.该方法适合环境水样的日常检测.

Abstract

An inductively coupled plasma mass spectrometer was used as the analytical instrument to establish the analytical methods for 13 metal elements in water.The results showed that:the calibration curves of the established method were linear with the correlation coefficients greater than 0.999;the detection limits were low,ranging from 0.01~0.26 μg/L;the relative standard deviations were small,all of them were less than 3%;and the accuracy was high,with the recoveries of spiked standards in the range of 92.3%~105.9%.The method is suitable for the routine testing of environmental water samples.

关键词

电感耦合等离子体质谱仪/金属元素/

Key words

inductively coupled plasma mass spectrometry/metal element/water

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出版年

2024
中国资源综合利用
徐州北矿金属循环利用研究所 中国物资再生协会

中国资源综合利用

CHSSCD
影响因子:0.358
ISSN:1008-9500
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