桑仁清肺口服液薄层鉴别检测方法优化研究
Qualiy Standard Improvement of Sangren Qingfei Oral Liquid TLC Identification
冯亚文 1刘德贤 2陈静 2李肖莉 1刘若男 3张娜 2张秋娜 3李会平 2郭莉 2刘佳2
作者信息
- 1. 河北省兽药饲料工作总站,石家庄 050000
- 2. 保定冀中药业有限公司,河北省中兽药技术创新中心,河北保定 071500
- 3. 保定冀中生物科技有限公司,河北保定 071000
- 折叠
摘要
为了提高桑仁清肺口服液质量标准,本研究改进甘草薄层鉴别方法.以甘草苷为对照,将供试品与对照品溶液点于同一1％氢氧化钠高效硅胶G薄层板上,乙酸乙酯-甲酸-冰醋酸-水(15∶1∶1∶2)为展开剂,10％硫酸乙醇溶液为显色剂.结果表明,1％氢氧化钠高效硅胶G薄层板展开效果良好.建立的甘草薄层鉴别方法专属性强,阴性无干扰,可用于桑仁清肺口服液甘草薄层鉴别.
Abstract
To improve the quality of standard of Sangren Qingfei oral liquid,this study improved the TLC identification method of Liquorice.Liquritn as the reference,the testing solution and the control solution were placed on the same 1％solution hydroxide efficient silica gel G plate,ethyl acetate/formic acid/glacial acetic acid and water(15∶1∶1∶2)as the developing solvent,vitriolic acid ethyl alcohol(10％)as color developing reagent.The results showed the 1％solution hydroxide efficient silica gel G plate had the best development effect.The established identification was exclusive,the negative control had no a interference,and could be used for the TLC identification of Liquorice.
关键词
桑仁清肺口服液/薄层鉴别/甘草/1％氢氧化钠高效硅胶G薄层板Key words
Sangren Qingfei oral liquid/TLC/liquorice/1％solution hydroxide efficient silica gel G plate引用本文复制引用
出版年
2024
国家科技期刊平台
NSTL
万方数据